UNITED STATES PATENT AND TRADEMARK OFFICE
`
`BEFORE THE PATENT TRIAL AND APPEAL BOARD
`
`
`ARKEMA INC. AND ARKEMA FRANCE
`Petitioner,
`v.
`
`HONEYWELL INTERNATIONAL INC.,
`Patent Owner.
`
`
`PGR2016-00011
`Patent No. 9,157,017
`
`
`PATENT OWNER’S SEVENTH AMENDED APPENDIX OF EXHIBITS
`
`
`
`
`
`
`
`
`

`

`PGR2016-00011
`
`Patent Owner’s Seventh Am. Appendix of Exhibits
`
`Exhibit No.
`
`Description
`
`Exhibit 2001
`
`Declaration of Donald Bivens
`
`Exhibit 2002
`
`Curriculum Vitae of Donald Bivens
`
`Exhibit 2003
`
`US. Patent No. 5,182,040 to Bartlett et al.
`
`Exhibit 2004
`
`US. Patent No. 5,516,446 to Bivens and Yokozeki
`
`Exhibit 2005
`
`US. Patent No. 5,648,017 to Bartlett et al.
`
`Exhibit 2006
`
`US. Patent No. 5,725,791 to Bivens et al.
`
`Exhibit 2007
`
`US. Patent No. 5,968,406 to Bartlett et a1.
`
`Exhibit 2008
`
`US. Patent No. 7,914,968 to Minor et a1.
`
`Exhibit 2009
`
`US. Patent No. 7,959,825 to Minor et al.
`
`Exhibit 2010
`
`Exhibit 2011
`
`Exhibit 2012
`
`Exhibit 2013
`
`Wilson, C. L. et al., Abstract: Man's Impact on the Global
`Environment: Assessment and Recommendation for Action.
`Report ofthe Study of Critical Environmental Problems (SCEP),
`MIT Press, Cambridge, Mass.
`(1970),
`available
`at:
`h . ://hdl.handle.net/1969.3/26655
`
`A. Hammond, Book Review of W. Matthews et al., Study of
`Man's Impact on Climate (SMIC) Report, Inadvertent Climate
`Modification, MIT Press, Cambridge, Mass. (1971), SCIENCE
`Vol. 176, available at: http://science.sciencemag.org/content/
`176/4030/38.2
`
`V- Ramanathan, Greenhouse Eflect Due to Chlorofluorocarbons:
`Climate Implications, SCIENCE: American Association for the
`Advancement of Science, Vol.
`190 (1975), available at:
`h o ://science.sciencema .or;
`
`J. Cahn and D. Didion., Trade-Ofifs in Refrigerant Selections:
`Past, Present,
`and Future, ASHRAE/NIST Refrigerants
`Conference October 1997
`
`
`
`Exhibit 2014
`
`B. Newell and T. Newell, In Situ, Real Time Oil Concentration in
`
`Exhibit 2015
`
`Exhibit 2016
`
`a Mobile Air Conditioning System, NI Tech Bulletin 001, Newell
`Instruments, Inc.
`
`ACURA Service Bulletin, R-I34a Refrigerant A/C System, Sept.
`29, 1992 for model NSX Le end, ear 1993
`
`2013 ASHRAE Handbook Fundamentals, SI Ed., Chapter 29:
`Refrierants, Table 3
`
`Exhibit 201 7
`
`Dometic, Material Safe Data Sheet, March 25, 2015
`
`Exhibit 201 8
`
`ICI Americas, Inc., FAG-46, Material Safety Data Sheet (Feb. 9,
`1999
`
`

`

`PGR2016-00011
`
`Patent Owner’s Seventh Am. Appendix of Exhibits
`
`Exhibit 2019
`
`Presentation, Exposure Limits: TL Vs, BEIs, PELs, RELs, WEELs,
`ERPGs
`and
`OELs,
`available
`online
`at:
`http ://isites.harvard.edu/fs/docs/icb.topic l 56420.files/Exposure_
`Limits
`
`Exhibit 2020
`
`US. Patent No. 6,516,837 to Thomas et al.
`
`Exhibit 2021
`
`Exhibit 2022
`
`Pate, Michael, et al., Miscibility 0fLubricants With Refrigerants,
`Final Report, Iowa State University of Science and Technology
`Deartment of Mechanical En ineerin; Jul 1993
`
`Crown, S.W., et al., A Comparison Study of the Thermal
`Performance ofR1 2 and R134a, International Refrigeration and
`Air Conditionin; Conference 1992
`
`Exhibit 2023
`
`Uemura, S., et al., Characteristics of HFC Refrigerants,
`International Refrigeration and Air Conditioning Conference
`
`
`
`Exhibit 2024
`
`Exhibit 2025
`
`Exhibit 2026
`
`Exhibit 2027
`
`Exhibit 2028
`
`Brown, J. Steven, et al., The fluorinated olefin R-I234ze(Z) as a
`high-temperature heatpumping refrigerant, International Journal
`of Refri_eration 32, 1412-1422 2009
`
`Case Law of the Board of Appeal of the European Patent Office
`Seventh Edition, Se I t. 2013
`
`Bristol Compressors, Medium and Low Temperature Retrofit
`fiom R502 to R404A/R507, Application Bulletin 125 (Release
`date Oct. 20, 1995
`
`Wilson, C. L. et al., Man’s Impact on the Global Environment:
`Assessment and Recommendation for Action. Report ofthe Study
`of Critical Environmental Problems
`(SCEP), MIT Press,
`Cambrid e, Mass. 1970
`
`Matthews, W., et al., Study ofMan’s Impact on Climate (SMIC)
`Report,
`Inadvertent Climate Modification, MIT Press,
`Cambrid e, Mass
`1971
`
`Seventh Edition, Se n t. 2013
`
`Exhibit 2030
`
`Exhibit 2031
`
`ASHRAE Standard, Designation and Safety Classification of
`Refrigerants, American Society of Heating, Refrigerating and
`Air-Conditionin_,
`.
`.
`,
`
`United States Environmental Protection Agency’s Office of
`Pesticide Programs, Summary of the IBT Review Program (July
`1983
`
`

`

`PGR2016-00011
`
`Patent Owner’s Seventh Am. Appendix of Exhibits
`
`Exhibit No.
`
`Description
`
`Exhibit 2032
`
`Exhibit 2033
`
`Manual for Investigation of HPV Chemicals, Chapter 3: Data
`Evaluation
`
`TSCA Filing, Refrigerant 1243zf; TNO Quality of Life Report: A
`sub-acute (28-day)
`inhalation toxicity study with 3, 3, 3,-
`tri uorouro-I—ene HFO 12342 in rats Dec. 3, 2010
`
`Exhibit 2034
`
`Clayton Jr., J. Wesley, Chapter 9: The Mammalian Toxicology of
`Or anic Comoounds Containin; Fluorine 1996
`
`Exhibit 2035
`
`US. Patent No. 5,569,797 to Fu et al.
`
`Exhibit 2036
`
`US. Patent No. 5,001,287 to Fernandez et al.
`
`Exhibit 2037
`
`ECETOC Technical Report No. 103: Toxicity of Possible
`Impurities and By-products in Fluorocarbon Products (December
`
`Exhibit 2038
`
`US. Patent A lication No. 13/939,233
`
`Exhibit 2039
`
`Transcript of Mar. 29, 2016 telephone proceedings before the
`Board
`
`Exhibit 2040
`
`Transcri it of Nov. 28, 2016 teleconference with the Board
`
`Exhibit 2041
`
`Transcri t of Nov. 29, 2016 teleconference with the Board
`
`Exhibit 2042
`
`US Patent Publication No. 2012/0292556 A1
`
`Exhibit 2043
`
`Exhibit 2044
`
`
`
`Exhibit 2045
`
`Beattie, Roger J., et al., Investigation of Low GWP Refrigerant
`Interaction with Various Lubricant Candidates,
`Purdue
`
`Exhibit 2046
`
`(2012),
`University
`. ://docs.lib_ urdue.edu/iracc/ 1223
`
`available
`
`at
`
`Domanski, Piotr A., et al., NIST, Transition to Low-GWP
`Refrigerants: Options and Tradeofifs, Florida International
`'
`' Aoril 1, 2016
`
`Exhibit 2047
`
`McLinden, Mark 0., NIST, Thermodynamic Analysis for Low-
`GWP Re ri ' erants, ASHRAE Winter Conference Jan. 19, 2014
`
`Exhibit 2048
`
`De osition Transcri ut of Dr. William J. Brock Dec. 1, 2016
`
`Exhibit 2049 D oosition Transcri t of Dr. J. Steven Brown Dec. 8, 2016
`
`Exhibit 2050
`
`Brown, J. Steven et al., Comparative analysis of an automotive
`air conditioning systems operating with C02 and R134a,
`International Journal of Refri eration 2002
`
`

`

`PGR2016-00011
`
`Patent Owner’s Seventh Am. Appendix of Exhibits
`
`Exhibit 2051
`
`Exhibit 2052
`
`Exhibit 2053
`
`Exhibit 2054
`
`Exhibit 2055
`
`Exhibit 2056
`
`Exhibit 2057
`
`Exhibit 2058
`
`Brown, Steven J., Potential R-114 Replacement Refrigerants,
`ASHRAE Transactions, Vol. 114 2008
`
`Clodic, Denis, Automobile Air-conditioning: Environmental
`Stakes and Future Technical Options, Journal of Cold and Air-
`conditionin 1
`
`Clodic, Denis, et al., Characteristics and Performances of New
`Re ri - erants, ADEME Technical Da
`Se t. 23 1999
`
`Ember, Lois R., et al., Tending the Global Commons, C&EN
`ov. 24, 1986
`
`EPA Approves New Coolant for Car AC Systems/Better climate
`protection without harming the ozone layer, available at
`. s:// osemitee .a.
`
`assessment
`Flammability
`al.,
`et
`Takizawa, Kenji,
`with
`fluoroalkenes
`CH2 =CFCF3.'
`Comparison
`uoroalkanes, Journal of Hazardous Materials 2009
`
`
`
`Exhibit 2059
`
`Kondo, Shigeo, et al., Flammability limits of olefinic and
`saturated fluoro-compounds, Journal of Hazardous Materials
`
`Exhibit 2060
`
`(Editor),
`Howe-Grant, Mary
`Comlrehensive Treatment 1995
`
`Fluorine
`
`Chemistry:
`
`A
`
`Exhibit 2061
`
`French Patent, No. 0 495 543 A1 1992
`
`Exhibit 2061A French Patent, No. 0 495 543 A1 1992 with certified translation
`
`Exhibit 2062
`
`of
`Toxicity
`Inhalation
`al.,
`et
`C.,
`Shayne
`Gad,
`Hexafluoroisobutylene, Toxicology and Applied Pharmacology
`March 31 1986
`
`Exhibit 2063
`
`GM First to Market Greenhouse Gas-Friendly Air Conditioning
`Refrigerant in US, available at: http://www-gm.com (July 23,
`
`Exhibit 2064
`
`Refrigerant Selection and System Design — the role of HFCs,
`Institute of Refrieration, Guidance Note 18 Aril 18, 2009
`
`Exhibit 2065
`
`US Patent Publication No- 201 1/03 1210] A1
`
`

`

`PGR2016-00011
`
`Patent Owner’s Seventh Am. Appendix of Exhibits
`
`Exhiblt 2066
`
`William L. Kopko, Beyond CFCs - Extending the Searchfor New
`Refrigerant, Proceedings of ASHRAE’s 1989 CFC Technology
`Conference 1989
`
`Exhibit 2066A William L. Kopko, Beyond CFCs - Extending the Searchfor New
`Refrigerant, Proceedings of ASHRAE’s 1989 CFC Technology
`Conference 1989
`
`Exhibit 2067
`
`McLinden, Mark 0., et al., Questfor Alternatives: A molecular
`approach demonstrates tradeoflis‘ and limitations are inevitable in
`seekin; re ri erants, ASHRAE Journal December 1987
`
`Exhibit 2067A McLinden, Mark 0., et al., Quest for Alternatives: A molecular
`approach demonstrates tradeofifs and limitations are inevitable in
`seekin ' re ri erants, ASHRAE Journal December 1987
`
`Exhiblt 2068
`
`Exhibit 2069
`
`Exhibit 2070
`
`Amendment and Response for Stable Formulated Systems with
`Chloro-3,3,3,-Tr1fluoropropene, US. Patent and Trademark
`Office, Serial No 12/667,121 Dec 29, 2009
`
`Amendment and Response for Heat Transfer of Oxygenated
`Lubricant with Hydrofluoroolefin and Hydrochlorofluoroolefin
`Refrigerants, US. Patent and Trademark Office, Serial No.
`14/715,753 Ma 19,2015
`
`Exhib1t2071
`
`Lindley, Andrew A., et al., Consideration ofHydrofluoroolefins
`
`Exhibit 2072
`
`(Inventor), Nearly Azeotropic Mixtures to Replace
`Jones, J.
`Refrigerant 12, NASA Tech Brief from JPL New Technology
`Reort,Vol 16 Au st 1992
`
`Exhibit 2072A Jones, J.
`
`(Inventor) Nearly Azeotropic Mixtures to Replace
`
`
`
`Exhibit 2073
`
`Exhibit 2074
`
`Exhiblt 2075
`
`Exhiblt 2076
`
`Brown, J. Steven, Preliminary Selection of R-114 Replacement
`Refrigerants Using Fundamental Thermodynamic Parameters
`
`Exhibit 2077
`
`U1
`
`

`

`PGR2016-00011
`
`Patent Owner’s Seventh Am. Appendix of Exhibits
`
`Exhibit No.
`
`Description
`
`Exhibit 2078
`
`US. Patent No. 6,258,292 Jul 10, 2001
`
`Exhibit 2079
`
`Exhibit 2080
`
`Exhibit 2081
`
`Suely,
`Carvalho,
`Hydrofluorocarbons,
`Develo ument
`
`to High-GWP
`al., Alternatives
`et.
`Institute for Governance & Sustainable
`
`Wang, Linda, Rajiv Singh Wins Schoellkopf Award, American
`Chemical Society, Chemical & Engineering News, Vol. 87, Issue
`12 March 23, 2009
`
`UNEP, 2002 Report of The Refrigeration, Air Conditioning and
`Heat Pumps, Technical Options Committee, Montreal Protocol
`On Substances that De 0 lete the Ozone La er 2002
`
`Exhibit 2082
`
`Exhibit 2083
`
`Fischer, S-K., et al., Energy and Global Warming Impacts ofCFC
`Alternative Technolo ies, AFEAS & DOE December 1991
`
`Specifications for Fluorocarbon Refrigerants, Air-Conditioning
`and Refi'i_eration Institute 2006
`
`Exhibit 2084
`
`Henne, Albert L., et. al., Fluorinated Derivatives ofPropane and
`Propylene, Department of Chemistry at the Ohio State University
`
`
`
`Exhibit 2085
`
`Exhibit 2086
`
`Haszeldine, R- N., Reactions ofFluorocarbon Radicals, Part V,
`Alternative Syntheses for Tn'fluoromethylacetylene (3:3 3-
`Trifluoropropyne), and the Influence of Pobzfluoro-groups on
`Adjacent Hydrogen and Halogen Atoms, University Chemical
`Laborato , Cambrid_e Atril 10, 1951
`
`P. L. Houston, Chemical Kinetics and Reaction Dynamics,
`Chapter 2: The Rates of Chemical Reactions (Apri117, 2000)
`(available
`h . ://www.cosbku _ atech.edu/y out/chem780/CHAPT2.
`
`Exhibit 2086A P. L. Houston, Chemical Kinetics and Reaction Dynamics,
`Chapter 2: The Rates of Chemical Reactions (Apri117, 2000)
`(available
`h o ://www.cosbkuo . _atech.edu/y ouo/chem780/CHAPT2.
`
`Exhibit 2087
`
`at
`(available
`textbook
`online
`Institute
`Keck Graduate
`http://sbw.kgi.edu/sbwwiki/_media/sysbio/labmembers/hsauro/s
`ystemsandsynthetic_biology3 .pdt)
`
`

`

`PGR2016-00011
`
`Patent Owner’s Seventh Am. Appendix of Exhibits
`
`Exhibit 2087A Herbert M. Sauro, Spring 2008: Systems and Synthetic Biology,
`1
`3
`Week
`,
`PowerPoint
`,
`http://sbw.kgi.edu/swaiki/_media/sysbio/labmembers/hsauro/s
`stemsands
`thetic biolo 3. odf.
`
`Exhibit 2089
`
`for Continued
`and Response with Request
`Amendment
`Prosecution by Arkema, Inc. re US. Patent Publication No.
`2011/0012052, Serial No. 12/667,140 Dec. 29, 2009
`
`Exhibit 2090
`
`US. Patent No. 5,152,845 Oct. 6, 1992
`
`Exhibit 2091
`
`Action on Ozone, Ozone Secretariat, United Nations Environment
`
`
`
`Exhibit 2092
`
`of
`
`Sciences,
`
`available
`
`at
`
`https://www.nap.edu/catalog/12024/energy-and-climate-studies—
`in-_eo.h sics 1977
`
`Exhibit 2093
`
`Didion, David A., et al., Role of refrigerant mixtures as
`alternatives to CFCs, Rev. Int. Froid, Vol. 13 Ma 13, 1990
`
`Exhibit 2094
`
`Declaration of Margaret H. Whittaker
`
`Exhibit 2095
`
`Exhibit 2096
`
`Directive 2006/40/EC of the European Parliament and of the
`Council Relating to emissions fiom air-conditioning systems in
`motor vehicles and amending Council, Directive 70/156/EEC,
`Official Journal of the Euro .ean Union Ma 17, 2006
`
`Klimisch, H.-J., et al., A Systematic Approach for Evaluating the
`Quality of Experimental Toxicological and Ecotoxicological
`lato Toxicolo and Pharmacolo
`1997 .
`
`Exhibit 2097
`
`Bhatti, M.S., A Critical Look at R- 744 and R-134a, Mobile Air
`
`Conditioning Systems, Reprinted from Automotive Climate
`Control Desi Elements SP-1239
`1997
`
`Exhibit 2098
`
`Arkema Beefs Up Chemicals; Eyes Acquisition ofAcrylics Assets,
`Chemical Week Business and Finance News 2008
`
`Exhibit 2098A Arkema Beefs Up Chemicals,“ Eyes Acquisition ofAcrylics Assets,
`Chemical Week Business and Finance News 2008
`
`Exhibit 2099
`
`VDA Annual Re D ort 201 1
`
`Exhibit 2100
`
`Recognizing our Heroes of Chemistiy, American Chemical
`Society, available at https://www.acs.org/content/acs/en/funding-
`and-awards/awards/indusn /heroes.html 2016
`
`

`

`PGR2016-00011
`
`Patent Owner’s Seventh Am. Appendix of Exhibits
`
`Exhibit 2101
`
`Declaration of Richard Winick, US. Patent and Trademark
`
`Office, In re Reexam Control Nos. 95/002,189 and 95/002,204,
`
`US. Patent No. 7,534,366 Filed Seot. 12, 2012
`
`Exhibit 2102
`
`Declaration of Richard Winick, US. Patent and Trademark
`
`Office, In re Reexam Control No. 95/002,030, US. Patent No.
`
`8,065,882
`
`'
`
`.
`
`,
`
`Exhibit 2103
`
`Declaration of Raymond Thomas, US. Patent and Trademark
`Office, In re Reexam Control Nos- 95/002,189 & 95/002,204,
`
`
`
`Exhibit 2104
`
`Exhibit 2105
`
`Exhibit 2106
`
`Exhibit 2107
`
`Exhibit 2108
`
`Exhibit 2109
`
`Exhibit 2110
`
`US. Patent No. 7,534,366 Filed Set. 12, 2012
`
`Schulze, Christian, et. al., Transient evaluation of a city bus air
`conditioning system with R-445A as drop-in -- From the
`molecules to the system,
`International Journal of Thermal
`Sciences 2015
`
`Li, Xinzhong, et. al-, Optimization ofHeat Exchangerfor
`High Glide Blend: Condenser model and its application in
`Oltimization or AC6 , SAE International Oct. 31, 2012
`
`Enrique Peral—Antl'mez (Chairperson), AJAC Refiigerant Blend
`Cooperative Research Program Update, SAE International (Oct.
`31, 2012
`
`Commercial CO2 Refrigeration Systems : Guide for Subcritical
`and Transcritical C02 Applications, Emerson Climate Study
`
`Chemours Congratulates the Parties to the Montreal Protocolfor
`HFC Amendment A reement, Chemours Article Oct. 17, 2016
`Honeywell Scientists Recognized As “Heroes of Chemistry ” For
`Development OfLow-Global- Warming Refi‘igerant , Honeywell
`Press Release June 17, 2016
`
`Exhibit 2111
`
`AI-IRI Past Pro ams -- 21CR Pro_ am, MCLR Pro am 2011
`
`Exhibit 2112
`
`Halocarbons: Environmental Efi'ects of Chlorofluoromethane
`Release, Committee on Impacts of Stratospheric Change,
`Assembly of Mathematical and Physical Sciences National
`Research Council, National Academ of Sciences 1976
`
`Exhibit 21 13
`
`Da
`
`1 D. DesMarteau Curriculum Vitae
`
`

`

`PGR2016-00011
`
`Patent Owner’s Seventh Am. Appendix of Exhibits
`
`Exhibit 2114
`
`Peroxide formation in glycol ethers, Dow Answer Center, The
`Dow
`Chemical
`Company,
`available
`at
`http://dowac.custhelp.com/app/answers/detail/a_id/ l 1446/~/pero
`xide-formation-in—l col-ethers
`ov. 15, 2011
`
`Exhibit 2115
`
`US. Patent No. 5,355,695 to Kawa; chi et al. Oct. 18, 1994
`
`Exhibit 2116
`
`Hudlicky, Milos, Organic Fluorine Chemistry, Dept. of
`Chemistry, Virginia Polytechnic Institute and State University
`
`Exhibit 2116A Hudlicky, Milos, Organic Fluorine Chemistry, Dept. of
`Chemistry, Virginia Polytechnic Institute and State University
`
`Exhibit 2117
`
`Amendments and Remarks to the Claims in Response to Office
`Action Mailed May 29, 2014,
`in re Patent Application No.
`
`
`
`Exhibit 2118
`
`Sealed Glass Tube Method to Test the Chemical Stability of
`Materials for Use within Refrigerant Systems, ASHRAE
`
`Exhibit 2119
`
`US. Patent No. 5,419,144 to Kawaguchi et al. (May 30, 1995)
`
`Exhibit 2120
`
`US. Patent No. 5,746,933 to Ishida et al. Ma 5, 1998
`
`Exhibit 2121
`
`US. Patent No. 6,299,792 B1 to Feirin_ et al. Oct. 9, 2001
`
`Exhibit 2122
`
`The Exponetial Growth of HF0-1234yf in Automotive Air
`Conditionin O teon YF The Chemours Coman 2016
`
`Exhibit 2123
`
`US. Patent
`
`o lication No. 2013/0296617 A1
`
`0v. 7, 2013
`
`Exhibit 2124
`
`Atiyeh, Clifford, Global Cooling: Mercedes to Debut Air
`Conditioning with C02 Refrigerant, Hearst Communications,
`
`Exhibit 2125
`
`Exhibit 2126
`
`Declaration of Donald Bivens December 15, 2016
`
`Exhibit 2127
`
`(General Editor), Hydrocarcons Halogenated
`Filov, V.A.
`Hydrocarbons, Harmful Chemical Substances Handbook (1990)
`
`Exhibit 2128
`
`Acute Toxici Data, RTECS 2016
`
`Exhibit 2129
`
`Huttenlocher, Dietrich F., Chemical and Thermal Stability of
`Refrigerant-Lubricant Mixtures with Metals, prepared for The
`Air-Conditioning and Refrigeration Technology Institute (Oct. 9,
`
`

`

`PGR2016-00011
`
`Patent Owner’s Seventh Am. Appendix of Exhibits
`
`Exhibit 2130
`
`Standard Test Method for Acid and Base Number by Color-
`
`Exhibit 213 1
`
`Exhibit 2 13 1A
`
`Exhibit 2 1 32
`
`
`
`Exhibit 2132A Chambers, Richard D., Fluorine in Organic Chemistry,
`Interscience Mono aihs on Or anic Chemist
`2004
`Chambers, Richard D., Fluorinin Or anic Chemist
`Chambers, Richard D., et al., Nucleophillic Reactions of
`Fluorinated Alkenes, Topics in Current Chemistry, Vol. 192
`
`Exhibit 2133
`Exhibit 2134
`
`Exhibit 2134A Chambers, Richard D., et al., Nucleophillic Reactions of
`Fluorinated Alkenes, Topics in Current Chemistry, Vol. 192
`
`Exhibit 2135
`
`Chambers, Richard D., et al., Reactions of Novel Unsaturated
`
`Exhibit 2135A Chambers, Richard D., et al., Reactions of Novel Unsaturated
`
`Exhibit 2 136
`
`Bartlett, Sheena, et al., Reactions Involving Flouride Ion, Part 20,
`Competition between Isomerization and Nucleophilic Attack on a
`
`Exhibit 2137
`
`Chambers Richard D., et al., Free Radical Chemistry, Part 9,
`Approaches to Fluorinated Polyethers Model Compound Studies
`
`Exhibit 2137A Chambers Richard D., et al., Free Radical Chemistry, Part 9,
`
`Exhibit 2138
`
`Chambers, Richard D., et al., Free-radical chemistry Part XII,
`Radical
`reactions of firfluoroethene,
`Journal of Flourine
`.
`'
`Aril 19, 2000
`
`Exhibit 2139
`
`al., Reactions of Fluoroolefins with
`et
`Dyatkin, B.L.,
`Electrophilic Reagents, Flourine Chemistry Reviews, Vol. 3
`
`Exhibit 2140
`
`HFO-1234yf encounters resistance as R-134a replacement for
`A/C, SAE International, available at http://articles.sae.org/8074/
`Aril 14, 2010
`
`10
`
`

`

`PGR2016-00011
`
`Patent Owner’s Seventh Am. Appendix of Exhibits
`
`Exhibit 2141
`
`Exhibit 2142
`
`Exhibit 2143
`
`Exhibit 2144
`
`Exhibit 2145
`
`Exhibit 2146
`
`Exhibit 2147
`
`Exhibit 2148
`
`Exhibit 2149
`
`Clayton Jr., J. Wesley, Fluorocarbon Toxicity and Biological
`Action, Toxici of Anesthetics 1967
`
`Clayton Jr., J. Wesley, The Mammalian Toxicology of Organic
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`Commandeur, J.N.M., et al., Nephrotoxicity and Hepatotoxicity
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`
`E.W. Cook and J.S. Pierce, Toxicology ofFluoro-olefins, Nature,
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`
`Kennedy In, G. L., Toxicology of Fluorine-containing
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`Potter, C .L., et al., Eflects ofInhaled Chlorotrzfluoroethylene and
`Hexafluoropropene on the Rat Kidney, Toxicology and Applied
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`
`Danishevskiy, S.L., et al., Toxicology of Some Fluoro-Organic
`Compounds, Foreign Technology Division (1989) - English
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`
`' l
`
`Exhibit 2149A Danishevskiy, S.L., et al., Toxicology of Some Fluoro—Organic
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`
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`
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`Final Test Results, Fluoroalkenes, EPA, Federal Register, Vol.
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`
`Shabecoff, Philip, EPA Threatens to Suspend Approval of
`Pesticides Over Test Flaws, The New York Times Jul 12, 1983
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`Exhibit 2152
`
`US. Patent Publication No. 2011/0001080 A1 Jan. 6, 2011
`
`Exhibit 2153
`
`Standard Test Methodfor An American National Standard Acid
`and Base Number by Color-Indicator Titration, ASTM
`International, Desi
`
`l
`
`

`

`PGR2016-00011
`
`Patent Owner’s Seventh Am. Appendix of Exhibits
`
`Exhibit 2154
`
`Protection of Stratospheric Ozone: Change ofListing Status for
`Certain Substitutes Under the Significant New Alternatives
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`
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`
`[Foreign Document] Vrednie Chemichescie Veshevsta,
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`
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`
`William B. Deichmann and Horace W. Gerarde, Toxicology of
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`
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`
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`
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`
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`
`EPA Health Effects Test Guidelines, Acute Inhalation Toxicity
`Au ; st 1998
`
`Papasavva, Stella, et al., Estimated 2017 Refrigerant Emissions
`of 2,3,3,3-tetrafluoropropene (HFC-I 234yfl in the United States
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`Science Technolo_ Oct. 26, 2009
`
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`Nephrotoxic Haloalkene
`I,1,2-Trichloro-3,3,3-Trifluoro-I-
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`
`Exhibit 2157
`
`Exhibit 2161
`
`Declaration of Dr. Da
`
`1 Desmarteau
`
`Exhibit 2162
`
`Office Action Summary, Application No. 14/225,588, US.
`Patent and Trademark Office Filed March 26, 2014
`
`Exhibit 2163
`
`US. Patent No. 7,084,315 B2 to Corr et. al. Au. 1, 2006
`
`Exhibit 2164
`
`Exhibit 2165
`
`Exhibit 2166
`
`US. Pat. App. No. 10/694,273
`Declaration of Ra'iv Sin h
`
`11—10-2008
`
`- Rule
`
`132
`
`Excerpts of Deposition Transcript of Dr. Raj iv R. Singh (Sep. 17,
`2011) from litigation in the Eastern District of Pennsylvania
`between Arkema and Hone
`ell, Civ. A. No. 2:10-cv—2886
`
`Exhibit 2167
`
`Declaration of Joseph Posillico in support of Patent Owner’s
`Motion for Leave to Reuest a Certificate of Correction
`
`12
`
`

`

`PGR2016-00011
`
`Patent Owner’s Seventh Am. Appendix of Exhibits
`
`Exhibit No.
`
`Exhibit 2168
`
`Description
`
`Patent Owner’s Proposed Request for a Certificate of
`Correction
`
`
`
`Exhibit 2169
`
`US. Provisional Patent A o o lication No. 60/693,853
`
`US. Patent A. slication No. 11/475,605
`
`US. Patent A. ulication No. 11/850,025
`
`US. Provisional Patent A. .lication No. 60/658,543
`
`Exce 0 ts of the Prosecution Histo of US. Patent No. 9,157,017
`
`Exhibit 2174
`
`for Certificate of Correction for US. Patent No.
`Request
`9,157,017
`
`13
`
`

`

`PGR2016-00011
`
`
`Date: May 6, 2020
`
`
`
`
`
` Patent Owner’s Seventh Am. Appendix of Exhibits
`
`Respectfully submitted,
`
`/s/ Noah Frank
`Gregg F. LoCascio, P.C. (Reg. No. 55,396)
`Noah Frank (Reg. No. 67,279)
`glocascio@kirkland.com
`noah.frank@kirkland.com
`KIRKLAND & ELLIS LLP
`1301 Pennsylvania Ave., N.W.
`Washington, DC 20004
`Telephone: (202) 389-5200
`Fax: (202) 389-5200
`Attorneys For Patent Owner
`
`
`
`14
`
`

`

`
`
`CERTIFICATE OF SERVICE
`The undersigned hereby certifies that a copy of the foregoing Patent Owner’s
`
`Seventh Amended Appendix of Exhibits and newly designated Exhibit 2174 were
`
`served on May 6, 2020, via electronic mail directed to counsel of record for the
`
`Petitioners:
`
`Mark D. Sweet
`
`Mark J. Feldstein
`
`Erin M. Sommers
`
`mark.sweet@finnegan.com
`
`mark.feldstein@finnegan.com
`
`erin.sommers@finnegan.com
`
`Charles W. Mitchell
`
`charles.mitchell@finnegan.com
`
`
`
`
`
`
`
`
`
`Arkema_PTAB@finnegan.com
`
`/s/ Noah Frank
`Noah Frank
`
`
`
`
`
`
`
`