`
`[11] Patent Number:
`6,072,237
`[191
`United States Patent
`[45] Date of Patent: *Jun. 6, 2000
`Jang et al.
`
`
`
`[54] BORDERLESS CONTACT STRUCTURE
`
`[75]
`
`Inventors: Syun-Ming Jang; Chen-Hua Douglas
`Yu, both of Hsin—Chu, Taiwan
`
`[73] Assignee: Taiwan Semiconductor
`Manufacturing Company, Hsin-Chu,
`Taiwan
`
`[*] Notice:
`
`This patent issued on a continued pros-
`ecution application filed under 37 CFR
`l.53(d), and is subject to the twenty year
`patent
`term provisions of 35 U.S.C.
`154(a)(2).
`
`[21] Appl. No.: 09/163,382
`
`[22]
`
`Filed:
`
`Sep. 30, 1998
`
`Related US. Application Data
`
`5,473,184 12/1995 Murai . . . . .. . .
`. . .. . . . .. 257/382
`
`5,497,022
`3/1996 Sakanioto ..
`257/377
`5,512,785
`4/1996 Haver et a1.
`..
`257/758
`5,521,409
`5/1996 Hsheh et al.
`..
`257/341
`
`5,523,616
`/1996 Den ............. ..
`257/637
`.. 257/649
`5,561,319
`10/1996 Owens et al.
`
`.. 257/382
`.
`5,736,770
`4/1998 Asai et al.
`
`257/377
`5,801,424
`9/1998 Luich ...........
`438/700
`1/1999 Dennison et a].
`5,858,877
`
`
`257/641
`5,880,519
`3/1999 Bothra et a1.
`4/1999 Lin ........................................ .. 257/758
`5,895,975
`
`FOREIGN PATENT DOCUMENTS
`
`405226334
`4060611361
`406163522
`
`9/1993
`3/1994
`/1994
`
`257/760
`Japan .................... ..
`
`257/760
`Japan ..
`Japan ................................... .. 257/760
`
`Primary Examiner—Mahshid Saadat
`Assistant Examiner—Edgardo Ortiz
`Attorney, Agent, or Firm—George O. Saile; Stephen B.
`Ackerman
`
`[62] Division of application No. 08/616,411, Mar. 15, 1996, Pat.
`No. 5,840,624.
`
`[57]
`
`ABSTRACT
`
`Int. Cl.7 ................................................... .. H01K 23/04
`[51]
`[52] US. Cl.
`........................ .. 257/698; 257/698; 257/760;
`438/634
`
`[58] Field of Search ................................... .. 257/698, 760;
`438/634
`
`[56]
`
`References Cited
`U.S. PATENT DOCUMENTS
`
`A method for forming a borderless, contact or via hole, has
`been developed, in which a thin silicon nitride layer is used
`as an etch stop to prevent attack of an underlying interlevel
`dielectric layer, during the opening of the borderless, contact
`or Via hole, in an overlying, interlevel dielectric layer. The
`thin silicon nitride layer is the top layer of an interlevel
`dielectric composite layer, used between metal interconnect
`levels.
`
`5,453,634
`
`9/1995 Mori ...................................... .. 257/316
`
`3 Claims, 6 Drawing Sheets
`
`
`
`7(N+) 5(N)
`
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`
`6
`
`18
`
`TSMC 1308
`
`TSMC 1308
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`
`
`US. Patent
`
`Jun. 6, 2000
`
`Sheet 1 0f 6
`
`6,072,237
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`
`
`
`10
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`FIG. 2 — Prior Art
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`US. Patent
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`Jun. 6, 2000
`
`Sheet 2 0f 6
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`6,072,237
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`US. Patent
`
`Jun. 6, 2000
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`Sheet 3 0f 6
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`6,072,237
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`Jun. 6, 2000
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`Sheet 4 0f 6
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`6,072,237
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`Jun. 6, 2000
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`Jun. 6, 2000
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`
`6,072,237
`
`1
`BORDERLESS CONTACT STRUCTURE
`
`This application is a divisional application of Ser. No.
`08/616,411, filed on Mar 15, 1996, and issued as US. Pat.
`No. 5,840,624, on Nov. 24, 1998.
`
`5
`
`BACKGROUND OF THE INVENTION
`
`(1) Field of the Invention
`The present invention relates to methods used to fabricate
`semiconductor devices, and more specifically to a process
`used to form Via holes.
`
`(2) Description of Prior Art
`The major objectives of the semiconductor industry has
`been to continually increase the device and circuit perfor-
`mance of silicon chips, while maintaining, or even
`decreasing, the cost of producing these same silicon chips.
`These objectives have been successfully addressed by the
`ability of the semiconductor industry to fabricate silicon
`devices, with sub-micron features. The ability to use sub-
`micron features, or micro-miniaturazation, has allowed per-
`formance improvements to be realized by the reduction of
`resistances and parasitic capacitances, resulting from the use
`of smaller features. In addition,
`the use of sub-micron
`features, results in smaller silicon chips with increased
`circuit densities,
`thus allowing more silicon chips to be
`obtained from a starting silicon substrate, thus reducing the
`cost of an individual silicon chip.
`The attainment of micro-miniaturazation has been basi-
`
`cally a result of advances in specific semiconductor fabri-
`cation disciplines, such as photolithography and reactive ion
`etching. The development of more sophisticated exposure
`cameras, as well as the use of more sensitive photoresist
`materials, have allowed sub-micron features in photoresist
`layers to be routinely achieved. In addition similar devel—
`opments in the dry etching discipline, has allowed these
`sub-micron images in photoresist layers, to be successfully
`transferred to underlying materials, used for the creation
`advanced semiconductor devices. However the use of sub-
`micron features, although improving silicon device perfor-
`mance and decreasing silicon chip cost, introduces specific
`semiconductor fabrication problems, not encountered with
`larger featured counterparts. For example, specific designs
`sometimes require that metal filled Via holes, in insulator
`layers, used to connect an overlying metallization structure
`to an underlying metallization structure, not always be fully
`landed. That is the metal filled Via, not being placed entirely
`on the underlying metallization structure. The inability to
`fully land a via on an underlying metal structure, places a
`burden on the process used to create the Via hole. For
`example if the chip design demands a non—fully landed, or
`a borderless contact, the dry etching procedure, used to
`create the via, has to be able to insure complete removal of
`insulator material from the area where the Via landed on the
`
`underlying metal structure, therefore necessitating the use of
`an overetch cycle. The overetch cycle however, can create
`problems in the area where the Via missed the underlying
`metal structure, and resided partially 011 an underlying
`insulator layer. The underlying insulator layer, may be
`identical, or similar, to the insulator used for the Via forma-
`tion. The extent of the Via hole overetch cycle can then result
`in severe etching of the underlying insulator layer, to a point
`where a lower level metallization structure may be exposed.
`Subsequent metal filling of the Via hole can then result in
`interlevel leakages or shorts. In addition the above phenom-
`ena can even occur, due to photolithographic misalignment
`situations, with fully landed contacts.
`
`10
`
`15
`
`r
`
`40
`
`45
`
`60
`
`65
`
`2
`in US. Pat. No. 5,350,712 describe a
`Shibata, et al,
`process for alleviating the consequences of the via hole
`misalignment, or borderless contact phenomena. However
`this present invention will describe a different approach to
`the misalignment or borderless contact, Via hole phenomena.
`An approach which offers protection from misalignment
`problems, with little added cost or complexity.
`
`SUMMARY OF THE INVENTION
`
`It is an object of this invention to fabricate silicon devices
`using metal filled Via holes that are not always fully landed,
`on underlying metal structures, as a result of a borderless
`contact design, or as a result of misalignment.
`It is another object of this invention to open a borderless
`contact, or misaligned via hole, in an overlying interlevel
`dielectric layer,
`to an underlying metal structure, while
`exposing a composite underlying interlevel dielectric layer
`in the area of misalignment, or in the area of borderless
`design at end point.
`It is still another object of this invention to use a com-
`posite underlying interlevel dielectric layer consisting of a
`top layer of insulator, that has a slower etch rate than the
`overlying interlevel dielectric layer.
`It is still yet another object of this invention to open the
`borderless, or misaligned Via,
`in the overlying interlevel
`dielectric layer, using a dry etching procedure, and being
`able to perform an overetch cycle to insure complete
`removal of the overlying interlevel dielectric layer, while not
`removing the top layer of the underlying, composite inter-
`level dielectric layer, in an area of misalignment, or border-
`less design.
`In accordance with the present invention a process is
`described for fabricating silicon devices using a borderless
`contact, or Via process,
`in which an etch stop layer is
`provided to protect underlying structures from attack during
`the borderless contact, dry etching process. A first, interlevel
`dielectric composite layer, comprised of a overlying thin,
`silicon nitride layer, and an underlying thick, silicon oxide
`layer, is deposited on an underlying metal structure, used to
`electrically contact an underlying active device region. A
`first Via hole is opened in the first interlevel dielectric
`composite layer, followed by deposition of a metallization
`layer, and patterning to form a metal structure. A second
`interlevel dielectric layer of silicon oxide is deposited on the
`underlying metal structure, as well as on the thin silicon
`nitride layer, of the first interlevel dielectric composite layer.
`A second via hole is opened, Via selective, dry etching
`procedures, in the second interlevel dielectric layer, expos-
`ing the top surface of the metal structure, and the surface of
`the thin silicon nitride layer, in regions where the borderless,
`or misaligned Via hole did not overlay the metal structure. A
`selective dry overetch procedure, used to insure complete
`removal of the second interlevel dielectric layer, from the
`surface of the metal structure, is performed without remov-
`ing the thin silicon nitride layer. The second via hole is then
`filled with a metal, and patterned to form another overlying
`metal structure.
`
`BRIEF DESCRIPTION OF THE DRAWINGS
`
`The object and other advantages of this invention are best
`described in the preferred embodiment with reference to the
`attached drawings that include:
`in cross-sectional style,
`FIG. 1, which schematically,
`shows an N channel MOSFET device, through contact level
`metal patterning.
`
`
`
`6,072,237
`
`3
`FIGS. 2—4, which schematically, in cross-sectional style,
`show prior art, and attempts at opening borderless contacts,
`or misaligned vias, to a first level metal structure, exposing
`an underlying contact level metal structure, in the region of
`via hole misalignment.
`FIGS. 5—8, which schematically, in cross sectional style,
`show the stages of fabrication used to create metal filled
`vias,
`in which the vias were of a borderless design, or
`misaligned, but did not result in exposure of underlying
`metal structures, during the dry etching procedure, due to the
`incorporation of a thin silicon nitride etch stop layer.
`DESCRIPTION OF THE PREFERRED
`EMBODIMENTS
`
`10
`
`15
`
`The method of fabricating via holes, using a borderless
`contact design, in which an etch stop layer is provided to
`protect against over etching and exposure of underlying
`metal structures, during the opening of the borderless
`contact, or via hole, will now be covered in detail. This
`invention can be used as part of metal oxide semiconductor '
`field effect transistors, (MOSFET), devices, that are now
`being manufactured in industry, therefore only the specific
`areas, unique to understanding this invention will be covered
`in detail. FIG. 1, schematically shows a typical N channel,
`(NFET), device, that this invention can be used with. A P ,
`type, substrate, 1, with a <100> crystallographic orientation,
`is used. Thick field oxide regions, 2, (FOX), are formed via
`conventional photolithographic and dry etching patterning
`of a composite insulator layer of silicon nitride and silicon
`dioxide, and then using the composite insulator layer as an
`oxidation mask, to thermally grow between about 4000 to
`6000 Angstroms of FOX insulator, 2,
`in the unmasked
`regions. After removal of the composite insulator, oxidation
`mask, a silicon oxide layer, 3,
`is thermally grown to a
`thickness between about 50 to 300 Angstroms, and used as
`the gate insulator of the MOSFET device. A polysilicon
`layer is next deposited, using low pressure chemical vapor
`deposition, (LPCVD), procedures, to a thickness between
`about 2000 to 4000 Angstroms, and doped via ion implan-
`tation of arsenic or phosphorous, at an energy between about
`50 to 100 Kev, at a dose between about 1E15 to 1E16
`atoms/cmz. The polysilicon layer is then patterned using
`conventional photolithographic and reactive ion etching,
`(RIE), processing, to create polysilicon gate structure, 4,
`shown schematically in FIG. 4.
`Alightly doped source and drain region, 5, is then formed
`via ion implantation of phosphorous at an energy between
`about 30 to 60 Kev., at a dose between about 1E12 to 5E13
`atoms/cmz. A layer of silicon oxide is deposited using either
`LPCVD or plasma enhanced chemical vapor deposition,
`(PECVD), processing, to a thickness between about 1500 to
`4000 Angstroms, and subjected to an anisotropic RIE
`procedure, in CHF3, to create insulator spacer, 6, shown in
`FIG. 1. A heavily doped source and drain region, 7, is then
`formed, via ion implantation of arsenic at an energy between
`about 50 to 100 Kev., at a dose between about 1E14 to 5E15
`atoms/cmz. Another silicon oxide layer, 8, is deposited using
`LPCVD or PECVD processing, at a temperature between
`about 400 to 800° C., to a thickness between about 3000 to
`6000 Angstroms, followed by a photolithographic and RIE
`procedure, using CHF3 as an etchant, and used to create
`contact hole, 9. After photoresist removal, using plasma
`oxygen ashing, followed by carefiil wet cleans, a metalliza-
`tion layer of aluminum, containing between about 1 to 3%
`copper, and between about 0.5 to 1% silicon, is deposited via
`r.f. sputtering, to a thickness between about 4000 to 8000
`Angstroms. The metallization layer can also be LPCVD
`
`40
`
`45
`
`60
`
`65
`
`4
`tungsten, deposited Via the decomposition of tungsten
`hexafluoride. Patterning of the metallization layer is per-
`formed by again using conventional photolithographic and
`RIE processing, using Cl2 as an etchant,
`to create metal
`structure, 10, shown schematically in FIG. 1. Photoresist
`removal is accomplished via plasma oxygen ashing followed
`by careful wet cleans.
`FIGS. 2—4, will show prior art, and attempts at creating
`borderless contacts, or misaligned Vias, to underlying metal
`structures, resulting in severe over etching of underlying
`insulators, due to the non-selectivity of the materials and dry
`etchants used. A layer of PECVD, silicon oxide, 11,
`is
`deposited at a temperature between about 400 to 600° C, to
`a thickness between about 3000 to 6000 Angstroms. A first
`via hole, 12, is created in silicon oxide layer, 11, to metal
`structure, 10, using conventional photolithographic and RIE
`processing, using CHF3 as an etchant. After photoresist
`removal, via plasma oxygen ashing and careful wet cleans,
`another metallization layer of aluminum, containing
`between about 1 to 3% copper, and between about 0.5 to 1%
`silicon is deposited using r.f. sputtering,
`to a thickness
`between about 4000 8000 Angstroms. This metallization
`layer can also be LPCVD tungsten, using a tungsten
`hexafluoride source, if desired. Patterning of the metalliza-
`tion layer, to form metal structure, 13, is accomplished again
`via conventional photolithographic and RIE procedures,
`using Cl2 as an etchant. FIG. 2, schematically shows this
`structure after photoresist removal using plasma oxygen
`ashing and careful wet cleans.
`An insulator layer of silicon oxide, 14, is deposited again
`using PECVD processing, at a temperature between about
`400 to 600° C., to a thickness between about 3000 to 6000
`Angstroms. The desired opening to metal structure, 13, is
`next addressed by opening a hole in photoresist layer, 15.
`The opening in photoresist layer can either be intentionally
`designed to be borderless, that is not open entirely on the top
`surface of metal structure, 13, or can suffer from misalign-
`ment problems, and again not open entirely over metal
`structure, 13. This is shown in FIG. 3. The dry etching
`procedure, used to open a second via, 16, in silicon oxide
`layer, 14, is next performed using CHF3 as an etchant. At the
`conclusion of the RIE procedure, or when end point is
`determined by the observance of the top surface of metal
`structure, 13, an additional overetch cycle is used to insure
`complete removal of silicon oxide, 14, from the top surface
`of metal structure, 13, in areas where poor uniformity of the
`PECVD silicon oxide layer, 14, may have existed. The
`overetch cycle does not adversely effect metal structure, 13,
`since the etchant used to create second via, 16, will not
`attack the metal. However the overetch cycle can severely
`attack the underlying silicon oxide layer, 11,
`in regions
`where the second via did not overlie metal structure, 13. The
`overetch creates a gouge or crevice, 17, shown schemati-
`cally in FIG. 4. The extent of this defect, when subsequently
`filled with an overlying metallization, can result in either
`deleterious leakage, or even shorts, between the overlying
`metallization and an underlying metal structure, used to
`electrically contact an active device region of the MOSFET
`structure, different
`then the active device region being
`addressed by a metal structure in second via, 16.
`A solution to the crevicing or gouging phenomena, occur-
`ring as a consequence of borderless contacts, or misaligned
`via holes, is now addressed. FIG. 5, again shows the creation
`of a metal structure, contacting both a polysilicon gate
`structure, 4, and a source and drain region, 7, through an
`opened contact hole, in silicon oxide layer, 8. The metalli-
`zation used is an underlying layer of titanium nitride,
`
`
`
`6,072,237
`
`5
`between about 200 to 500 Angstroms, a layer of aluminum,
`between about 4000 to 8000 Angstroms, containing between
`about 1 to 3% copper, and between about 0.5 to 1% silicon,
`and an overlying layer of titanium nitride, again between
`about 200 to 500 Angstroms. The titanium nitride layers
`offer, adhesive, barrier, and electromigration enhancements.
`The metallization layer is then patterned using conventional
`photolithographic and RIE procedures, using Cl2 as an
`etchant to create metal structure, 18. Photoresist removal is
`performed using plasma oxygen ashing and careful wet
`cleans. A composite interlevel dielectric layer is then
`deposited, consisting of an underlying silicon oxide layer,
`19, obtained via PECVD processing, at a temperature
`between about 400 to 600° C., to a thickness between about
`3000 to 6000 Angstroms, and an overlying layer of silicon
`nitride, 20, obtained Via PECVD processing, at a tempera-
`ture between about 400 to 600° C., to a thickness between
`about 500 to 1000 Angstroms.
`A first via hole, 21,
`is next opened in the composite
`interlevel dielectric layer,
`to expose metal structure, 18,
`which in turn is contacting an underlying polysilicon gate
`structure, 4, Via use of conventional photolithographic and
`RIE procedures, using Cl2 for silicon nitride layer, 20, and
`CHF3, for silicon oxide layer, 19, as etchants. After removal
`of photoresist via plasma oxygen ashing and careful wet
`cleans, another layer of titanium nitride—aluminum, with
`copper and silicon,—titanium nitride,
`is deposited using
`process conditions, and film thicknesses, identical to those
`previously supplied for the metallization layer used to create
`metal structure, 18. Photolithographic and RIE procedures,
`again using Cl2 as an etchant are used to define metal
`structure, 22, shown schematically in FIG. 6. Photoresist
`removal is again accomplished using plasma oxygen ashing
`and careful wet cleans.
`
`is deposited using PECVD
`A silicon oxide layer, 23,
`processing, at a temperature between about 400 to 600° C.,
`to a thickness between about 3000 to 6000 angstroms.
`Photoresist layer, 24, is applied and exposed to open a region
`to be used for an intentional borderless contact. The opening
`may be also be misaligned, which will create an uninten-
`tional borderless contact. A RIE procedure is next used to
`open second via hole, 25, in is silicon oxide layer, 23. The
`chemistry of the etchant used, CHF3 for silicon oxide layer,
`23, and the RIE conditions are chosen to result in a selec-
`tivity of silicon oxide layer, 23, to underlying silicon nitride
`layer, 20, of between about 3 to 1, in the CHF3 ambient. The
`enhanced selectivity between silicon oxide and the under-
`lying silicon nitride layer, allows a robust overetch cycle to
`be performed to insure complete removal of thick regions of
`silicon oxide from the top surface of metal structure 22,
`without creating a severe gouge or crevice in the underlying
`composite interlevel dielectric layer, in regions where the
`second via, 25, did not overlie metal structure, 22. The
`minimum crevice or gouge, 26, is confined to the thin silicon
`nitride etch stop layer, 20. This is schematically shown in
`FIG. 7. Photoresist removal
`is performed using plasma
`oxygen ashing and careful wet cleans.
`Another metallization is performed via r.f. sputtering, of
`overlying and underlying layers of titanium nitride, at a
`thickness between about 200 to 500 Angstroms, and a core
`layer of aluminum, containing between about
`1 to 3%
`copper, and between about 0.5 to 1% silicon, at a thickness
`between about 4000 to 6000 Angstroms. Once again pat-
`terning of the metallization layer is accomplished via stan-
`dard photolithographic and RIE procedures, using Cl2 as an
`etchant, to create metal structure, 27. Photoresist removal is
`again performed using plasma oxygen ashing, followed by
`
`10
`
`15
`
`V
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`,
`
`40
`
`45
`
`60
`
`65
`
`6
`careful wet cleans. FIG. 8, schematically shows that silicon
`nitride etch stop layer, 20, preventing crevicing or gouging
`of silicon oxide layer, 19, and thus prevented leakage or
`shorts between metal structure, 27, connected to a polysili-
`con gate structure, and metal structure, 18, connected to a
`source and drain region, of a MOSFET device structure.
`Although this process for creating borderless contacts,
`using a silicon nitride etch stop, to prevent metal leakages
`and shorts, has been shown for an N channel, (NFET)
`device, it can also be applied to P channel, (PFET), devices,
`complimentary, (CMOS), devices, as well as to BiCMOS
`devices.
`
`While this invention has been particularly shown and
`described with reference to,
`the preferred embodiments
`thereof, it will be understood by those skilled in the art that
`various changes in form and details may be made without
`departing from the spirit and scope of this invention.
`What is claimed is:
`1. A MOSFET device structure, with a borderless contact
`structure, on a semiconductor substrate, featuring a notch, in
`a thin silicon nitride stop layer, protecting the integrity of an
`underlying insulator layer, while insuring complete sidewall
`contact of said borderless contact structure, to an adjacent
`metal structure, comprised of:
`field oxide regions in said semiconductor substrate;
`a device region between said field oxide regions;
`a first polysilicon gate structure in center of said device
`region, and a second polysilicon gate structure on a first
`field oxide region;
`a source and drain region in said device region, located
`between said first field oxide region, and said first
`polysilicon gate structure;
`a first insulator layer on said field oxide regions, on said
`source and drain region, on said first polysilicon gate
`structure, and on said second polysilicon gate structure;
`a contact hole in said first insulator layer, exposing a
`portion of the top surface of said second polysilicon
`gate structure;
`a contact level metal structure, comprised of a first portion
`of said contact level metal structure, completely filling
`said contact hole,
`in said first insulator layer, and a
`second portion of said contact level metal structure,
`located on said first insulator layer;
`a composite, second insulator layer, comprised of said
`thin silicon nitride, stop layer, overlying a thick silicon
`oxide, underlying layer, located on said second portion
`of said contact level metal structure, and on the portion
`of said first insulator layer, not covered by said second
`portion of said contact level metal structure;
`a first via hole in said composite, second insulator layer,
`exposing a portion of the top surface of said second
`portion of said contact level metal structure;
`a first level metal structure, comprised of a first portion of
`said first level metal structure, completely filling said
`first via hole, and a second portion of said first level
`metal structure,
`located on the top surface of said
`composite, second insulator layer;
`a third insulator layer, located on second portion of said
`first level metal structure, and on the portion of said
`composite, second insulator layer, not covered by said
`second portion of said first level metal structure;
`a bordcrlcss via hole comprised of; a first portion of said
`borderless via hole,
`in a top portion of said third
`insulator layer, exposing a portion of the top surface of
`said second portion of said first level metal structure;
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`
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`6,072,237
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`7
`and a second portion of said borderless via hole, in said
`third insulator layer, and in a top portion of said thin
`silicon nitride stop layer, featuring said notch in the top
`portion of said thin silicon nitride stop layer, and with
`said second portion of said borderless Via hole exposing
`a complete side of said second portion of said first level
`metal structure; and
`said borderless contact structure, comprised of a first
`portion of said bordcrlcss via holc structure, complctcly
`filling said first portion of said borderless via hole, and
`completely filling said second portion of said border-
`less via hole contacting the complete side of said
`second portion of said first level metal structure, and
`contacting the top portion of said second portion of said
`
`5
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`10
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`8
`first level metal structure, exposed in said borderless
`via hole, and comprised of a second portion of said
`bordcrlcss contact structure, ovcrlying a portion of the
`top surface of said third insulator layer.
`2. The MOSFET device structure of claim 1, wherein said
`composite, second insulator layer, is comprised of an over-
`lying layer of silicon nitride, between about 500 to 1000 in
`thickness, and an underlying layer of silicon oxide, between
`about 3000 to 6000 Angstroms in thickncss.
`3. The MOSFET device structure of claim 1, wherein said
`third insulator layer is silicon oxide, between about 3000 to
`6000 Angstroms in thickness.
`*
`*
`*
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`*
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`*
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`