`
`= Aurora
`
`‘qlllAnalytics
`
`Innovative Chemistry. Neoteric Solutions.
`
`Certificate of Analysis
`
`
`Product Name:
`Product Number:
`
`Compound 13 Darunavir
`
`Lot Number:
`
`C13-040215-2
`
`Amount:
`Chemical Name:
`
`CAS Number:
`
`0.5 g
`[(1 S,2R)-3-[[(4-aminophenyl)sulfonyl](2-methylpropyl)amino]-2-
`hydroxy-l - (phenylmethyl)propyl]—carbamic acid (3R,3aS,6aR)-
`hexahydrofuro[2,3-b]furan—3-yl ester
`20631-99—1
`
`Chemical Formula:
`
`C27H37N307$
`
`Molecular Weight:
`
`547.66 gfmole
`
`Structure:
`
`CH3
`
`Compound 13, Darunavir
`
`
`
`
`Appearance:
`Off-white glassy solid
`Purity (HPLC-UV254):
`9?%
`
`Mp (°C, uncorrected)
`77-78 °C
`
`NMR (CDC13)
`Consistent with expected structure
`
`LRMS (ESI+)
`Consistent with molecular formula
`Solubility:
`EtOAc, DCM, ethanol
`
`TLC (Silica gel 60 F254)
`
`Stora e:
`
`
`
`
`Certified by:
`
`a E
`
`:
`
`Chief Operating Officer
`
`Date:
`
`‘7 Z 5 g [5
`
`Aurora Analytics: LLC
`1450 South Rolling Road
`Baltimore, MD 2 l227
`
`Phone: 443-543-5799
`FAX: 443-543-5790
`aka]ivret@auroraanalytics.com
`Lupin Ex. 1089 (Page 1 of 1)
`Lupin Ex. 1089 (Page 1 of 1)
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