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`ParticleTrack G400
`Real-Time Particle Characterization
`
`Operating Instructions
`Hardware Manual
`
`

`

`Downloaded from www.Manualslib.com manuals search engine
`
`This publication may contain or reference
`information and products protected by copyrights
`or patents and do not convey any license under
`the patent rights of Mettler-Toledo AutoChem, Inc.,
`nor the rights of others. Mettler-Toledo AutoChem,
`Inc. does not assume any liability arising out of
`any infringements of patents or other rights of third
`parties.
`
`Mettler-Toledo AutoChem, Inc. makes no warranty
`of any kind with regard to this manual, including
`but not limited to the implied warranties of
`merchantability and fitness for a particular purpose.
`
`04192016
`
`No part of this publication may be stored in a
`retrieval system, transmitted, or reproduced in
`any way, including but not limited to photocopy,
`photograph, magnetic or other record, without
`the prior written permission of Mettler-Toledo
`AutoChem, Inc.
`
`FBRM®, iC Process™, iC FBRM™, PVM™, and
`iC PVM™ are trademarks of Mettler-Toledo
`AutoChem, Inc.
`
`Microsoft® and Windows® are either registered
`trademarks or trademarks of Microsoft Corporation
`in the United States and/or other countries.
`
`All other brand and product names are trademarks
`or registered trademarks of their respective owners.
`
`The information in this publication is provided for
`reference only. All information contained in this
`publication is believed to be correct and complete.
`Mettler-Toledo AutoChem, Inc. shall not be liable
`for errors contained herein nor for incidental or
`consequential damages in connection with the
`furnishing, performance, or use of this material. All
`product specifications, as well as the information
`contained in this publication, are subject to change
`without notice.
`
`For technical support, email: AutoChemCustomerCare@mt.com
`For updates, webinars, and the latest documents: http://community.autochem.mt.com
`Mettler-Toledo AutoChem, Inc.
`7075 Samuel Morse Drive
`Columbia, MD 21046
`www.mt.com/AutoChem
`Tel: + 1 866.333.6822
`Fax: +1 410.910.8600
`
`2
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`Hardware Manual
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`Contents
`
` 1 Introduction
`
` 2 Intended Use
`
` 3 Technical Data
`
` 4 Safety Information
`
` 5 Supplementary Documentation
`
` 6 Product Installation
`
` 7 Probe Mounting Options
`
`8 Operating Instructions
`
` 9 Best Practices for Routine Operation
`
`10 Troubleshooting
`
`11 Product Maintenance
`
`12 Disposal
`
`1
`
`Introduction
`This manual covers specific safety and quality information relating to the
`ParticleTrack™ G400 with FBRM® (Focused Beam Reflectance Measurement) technology.
`Throughout this manual, the system is referred to by the name: ParticleTrack G400 or
`FBRM G400. The ParticleTrack G400 system includes the base unit and probe connected
`by a flexible armored conduit.
`
`ParticleTrack G400 is a probe-based instrument that is inserted directly into laboratory
`reactors to track changing particle size and count in real time at full process
`concentrations. Particles, particle structures, and droplets are monitored continuously,
`as process parameters vary, providing scientists with the evidence required to deliver
`consistent particles with the required attributes. A ParticleTrack G400 system has fixed
`or interchangeable probe options and includes options for a single or dual-system
`configuration. ParticleTrack G400 dual-system configurations can simultaneously
`measure two small-scale vessels or points in a process stream. Click the link to see the
`FBRM Method of Measurement video (requires internet connection).
`
`www.mt.com/ParticleTrack G400
`
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`2
`
`Intended Use
`The system includes a power supply, laser and detector modules, and PCBs. The base
`unit is fitted with a permanently attached flexible armored conduit, which is connected to
`the process probe. The ParticleTrack G400 system is designed for indoor use.
`The system may only be used in safe locations and is not certified for use in hazardous
`locations.
`
`3 Technical Data
`
`System certifications
`
`CE/NRTL-C Approved, Class 1 Laser Device, Compliant
`with 21CFR1040.10 and 1040.11 and IEC 60825-1; IPX0
`
`Functional specifications
`Method of Measurement
`Measurement range
`Scan speed
`
`Focused Beam Reflectance Measurement (FBRM®)
`0.5 to 2,000 µm
`2 m/s (14 mm probe: 125 Hz)
`1.2 m/s (19 mm probe: 75 Hz)
`
`Table 1. System certifications and functional specifications
`
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`91 mm
`[3.6”]
`
`199 mm
`[7.83”]
`
`Base Unit Specifications
`
`9.5 mm
`[Ø 0.38”]
`
`32 mm
`[Ø 1.25”]
`
`241 mm
`[9.5”]
`
`Power On
`
`Communication
`
`HW Status
`
`SW Status
`
`89 mm
`[3.5”]
`
`492 mm
`[19.4”]
`
`Figure 1. System Dimensions—Base unit
`
`Environmental
`Operating humidity range
`Operating temperature range
`
`0 to 85%
`5 to 35 °C
`
`General
`Material of construction
`
`Ingress protection
`Power
`Weight
`Communication interface
`Pollution degree
`Installation (overvoltage) category
`PCBs
`
`Table 2. Base unit specifications
`
`14 ga Aluminum
`with Class 3 RoHS-compliant chemical film
`IPX0
`100-240 VAC, 50/60 Hz, 1.2A
`3.25 kg [7.17 lb]
`USB, 3 m [10 ft] cable
`2
`II
`Fr–4
`
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`[15.57”]
`
`[7.83”]
`
`19 mm
`Probe Specifications
`[Ø 0.75”]
`
`70 mm
`[2.76”]
`
`136 mm
`[5.35”]
`
`32 mm
`[Ø 1.25”]
`
`199 mm
`[7.83”]
`
`9.5 mm
`[Ø 0.38”]
`
`14 mm
`[Ø 0.55”]
`
`32 mm
`[Ø 1.25”]
`
`Figure 2. Probe dimensions—G400 14 mm probe
`
`91 mm
`[3.6”]
`
`9.5 mm
`[Ø 0.38”]
`
`400 mm
`[15.57”]
`
`19 mm
`[Ø 0.75”]
`
`241 mm
`Figure 3. Probe dimensions—G400 19 mm probe
`[9.5”]
`70 mm
`136 mm
`[2.76”]
`[5.35”]
`14/9.5 mm
`
`Power On
`
`199 mm
`[7.83”]
`199 mm
`[7.83”]
`
`32 mm
`[Ø 1.25”]
`
`32 mm
`[Ø 1.25”]
`
`199 mm
`[7.83”]
`19 mm
`
`Communication
`
`HW Status
`
`SW Status
`
`Wetted materials of
`construction
`Probe tip
`Probe window
`Probe window seals
`
`89 mm
`[3.5”]
`
`9.5 mm
`[Ø 0.38”]
`
`14 mm
`Alloy C22
`[Ø 0.55”]
`Sapphire
`492 mm
`[19.4”]
`TM [Thermo-Mechanical
`press-fit] (standard)
`91 mm
`[3.6”]
`
`32 mm
`Alloy C22
`[Ø 1.25”]
`Sapphire
`Kalrez® 6375 (standard)
`TM [Thermo-Mechanical
`199 mm
`[7.83”]
`press-fit] (optional)
`
`Environmental
`Operating pressure range *
`
`Operating temperature range
`241 mm
`[9.5”]
`
`32 mm
`9.5 mm
`3 barg (standard)
`[Ø 0.38”]
`[Ø 1.25”]
`0 to 100 barg (optional, requires custom engineering design)
`+10 to 90 °C (standard)
`–80 to 90 °C (TM seal and purge)
`–10 to 90 °C (Kalrez® seal and purge)
`
`Power On
`
`Communication
`
`Installation
`Conduit length
`Conduit diameter
`Conduit bend radius (min.)
`Probe and conduit weight
`
`HW Status
`
`SW Status
`
`89 mm
`3 m [9.8 ft]
`[3.5”]
`11.6 mm [0.46 in]
`12.7 cm [5 in]
`492 mm
`1.36 kg [3 lb]
`[19.4”]
`
`3 m [9.8 ft]
`11.6 mm [0.46 in]
`12.7 cm [5 in]
`1.81 kg [4 lb]
`
`* Note: Probe operating temperatures below the dew point temperature of the environment
`require purge air, described on page 11.
`
`Table 3. Probe specifications
`
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`Site preparation for the METTLER TOLEDO ParticleTrack G400 system is the end
`user's responsibility. The following should be considered to ensure successful system
`installation:
`
`Power Requirements
`
`Verify that a power outlet is accessible in the area of intended use for the
`ParticleTrack G400. Provide one outlet for a single system or two outlets for a dual-
`system configuration.
`
`Area of Intended Use
`
`The area of intended use must provide adequate space for the base unit, conduit and
`probe. The probe conduit should not bend beyond 12.7 centimeters (5 inches) and it
`should not be put into an “S” shape. The base unit must be convenient for access at eye
`level to view the LED status indicators; readily accessible for service; securely placed
`horizontally on a flat surface; and installed in an area that has access to instrument
`quality air (when operating below the dew point, purge gas is to be connected to the rear
`of the instrument). The ParticleTrack G400 system enclosure contains sensitive electronic
`components that should be protected from severe environmental conditions. Direct,
`intense sunlight can raise the internal temperatures above operating specifications. Refer
`to section "3 Technical Data" starting on page 4, for the temperature and humidity
`specifications of the base unit, and the system size and weight specifications.
`
`Air/Gas Requirements (if applicable)
`To prevent condensation when operating below the dew point of the environment,
`ParticleTrack G400 probes require a source of clean, dry, and pressure-regulated
`instrument air or inert gas. The quality of the air or gas supply must meet the
`specifications of the American National Standards Institute/Instrument Society of America
`(ANSI/ISA) S7.0.01-1996 Quality Standard for Instrument Air. Air/gas must:
`• Have a dew point at least 10 °C [50 °F] lower than the minimum temperature to
`which any part of the system will be exposed.
`• Contain less than 1 ppm total oil or hydrocarbons
`• Contain less than 1 ppm particulates at a maximum size of 3 microns
`• Be free of any corrosive contaminants and flammable or toxic gases.
`
`Air supply pressure, maximum
`Operating pressure, normal
`Pre-purge for one (1) hour
`Operating flow rate
`
`Table 4. Probe air/gas specification
`
`8.6 barg [125 psig]
`1.0 barg [15 psig]
`1.2 SLPM [0.042 SCFM]
`0.15 SLPM [0.005 SCFM]
`
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`4 Safety Information
`
`The CE Mark applies only to unmodified instruments as supplied by
`Mettler-Toledo AutoChem, Inc. Modifications may require on-site testing for
`compliance verification. If the equipment is used in a manner not specified
`by the manufacturer, the protection provided by the equipment may be
`impaired.
`Caution—Read all safety warnings before installing or operating this
`equipment. Failure to follow the instructions and caution/warning
`statements could result in personal injury and/or product damage that
`could void the warranty.
`
`WARNING—This equipment shall be connected to mains socket outlet with
`a protective earthing connection.
`
`WARNING—This equipment is approved for indoor use only.
`
`Table 5. Safety cautions and warnings
`
` Laser Classification
`
`All standard-model FBRM G400 instruments are in compliance with the U. S. Department
`of Health and Human Services (DHHS) Radiation Performance and in accordance with
`International Standards.
`THE FBRM G400 IS A CLASS 1 LASER PRODUCT COMPLIANT WITH
`DHHS 21 CFR 1040.10 AND 1040.11
`EXCEPT FOR DEVIATIONS PURSUANT TO LASER NOTICE 50, DATED JUNE 24, 2007.
`THE FBRM G400 IS A CLASS 1 LASER PRODUCT COMPLIANT WITH IEC 60825-1
`Laser de Classe 1
`Conforme à la norme 21 CFR 1040.10 et 1040.11
`À l'exception des écarts conformement à l'avis Laser 50 en date du 24 Juin 2004
`et conforme à la norme IEC 60825-1
`
`LASER SAFETY WARNING
`Opening the enclosure and making adjustments, or performing procedures
`other than those specified in the instrument manual may result in
`hazardous radiation exposure.
`
`Caution—Use of controls or adjustments or performance of procedures
`other than those specified in the instrument manual may result in
`hazardous radiation exposure.
`
`There are no user-serviceable components in the laser module. Only
`skilled, trained technicians can service this equipment.
`
`Looking directly into the aperture of any laser-emitting device is never
`advised.
`
`Table 6. Laser safety warnings and cautions
`
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`5 Supplementary Documentation
`An electronic ParticleTrack G400 Hardware Documentation Portfolio, shipped with the
`instrument, includes the following documents in addition to this manual:
`
`• Quick Ref: “Positioning the ParticleTrack or ParticleView Probe” (MK-PB-0050-AC)
`
`• “Calibration Validation in iC FBRM” (MK-PB-0071-AC)
`
`• “System Calibration in iC FBRM” (MK-PB-0082-AC)
`
`• QuickRef: "Changing ParticleTrack G400 Interchangeable Tips” (MK-PB-0080-AC)
`
`• QuickRef: “Using the PSC Purge Controller” (MK-PB-0120-AC)
`
`Please refer to the iC FBRM software user assistance and Documentation Portfolio for
`software publications.
`Check the http://community.autochem.mt.com site for the latest portfolios.
`
`6 Product Installation
`ParticleTrack G400 system installation involves two connections to the power and USB
`communication inlets at the back of the base unit. If the optional purge controller is
`purchased, a third connection to instrument-quality air is also on the back of the unit. For
`dual-system configurations, note that the procedure is to connect and configure the first
`system entirely. Then, connect and configure the second system. System connections are
`completed by a METTLER TOLEDO qualified Field Service Engineer. Connection details are
`provided below should the system be relocated following the initial installation.
`
`Due to the complex nature of multi-phase flow, proper installation is very important for
`successful application of inline particle and droplet measurement techniques. Installation
`and mounting of probe-based instruments for particle characterization should consider
`multiple factors including:
`
`• Existing or planned laboratory or process equipment
`
`• Expected ranges of process variables such as temperature, pressure, flow rates, and/
`or flow patterns
`
`• Expected range of particle/droplet size and concentration
`
`• Probe location and orientation as shown in Figure 4.
`
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`A
`
`B
`
`C
`
`D
`
`Figure 4. Implementation of a ParticleTrack instrument: (A) flush with wall of vessel or pipeline; (B) inserted
`tangentially to process flow; (C) inserted perpendicular to process flow at an elbow; and (D) inserted at
`optimal angle (45°) relative to process flow
`
`Connect Power (A, B)
`1. Connect the pin-terminated end of the country-specific, auto-switching AC Power
`Adapter (B) to the Power connection (A) at the back of the ParticleTrack G400 base
`unit (Figure 5).
`2. Connect the opposite end to an AC outlet.
`3. Press the power button on the front of the ParticleTrack G400 base unit and observe
`that the Power LED indicator illuminates.
`4. Ensure the ParticleTrack G400 system has been powered ON for 30 minutes before
`performing calibration validation or recording particle system measurements.
`
`USB
`
`C
`
`A D
`
`Air/Inert gas (optional)
`
`B
`
`Figure 5. Instrument connections: (A) Power input (B) Switching AC Adapter; (C) USB
`communications; (D) Air/inert gas (if applicable)
`
`Connect USB Communications (C)
`1. Connect the USB cable to the first input (C) at the back of the ParticleTrack G400
`base unit.
`2. Connect the other end of the cable to a USB port on the control computer.
`Note: The Communications LED on the front of the base unit will not illuminate
`permanently until the software connection is complete.
`
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`Optional: Connect Air Supply (D)
`
`When operating below the dew point temperature of the environment, purge air is
`required. The Purge Controller should be used to regulate the purge air flow.
`
`1. Clean/purge all air lines and tubes before connecting to the ParticleTrack G400
`instrument.
`
`2. Connect the air supply to the air inlet
`on the Purge Controller. The required
`tubing from the air supply, to the Purge
`Controller is user-supplied (6.35 mm
`[1/4-inch], rated for 120 psig, may be
`made of polypropylene, PVC, or nylon).
`
`3. Connect the purge tubing (6 mm [0.23
`inch], supplied with Purge Controller)
`to the purge fitting on the rear of the
`ParticleTrack G400 base unit, near the
`probe conduit connection (D in Figure 5).
`
`4. Adjust the Purge Controller pressure
`and set it to the pre-purge flow rate
`for one hour (Table 4). After the one
`hour pre-purge, set the purge flow rate
`to the operating flow rate to run an
`experiment.
`
`5. Refer to the quick reference guide
`for further details—"QuickRef-Using
`the PSC Purge Controller" (MK-PB-
`0120-AC).
`Note: The probe exhaust holes for
`purge air are located at the top of the
`probe, just below the retaining nut
`(Figure 7).Take care during installation
`and cleaning of the probe to ensure
`the exhaust holes are not blocked or
`submerged in liquid.
`
`Figure 6. Purge Controller
`
`Figure 7. Probe exhaust (one of three)
`
`7 Probe Mounting Options
`
`ParticleTrack G400 probes are specifically designed for mounting in small reactors such
`as the METTLER TOLEDO EasyMax™ or OptiMax™.
`
`Lab-joint adapters are manufactured from PTFE (polytetrafluoroethylene) with O-ring
`seals, and designed for the installation of ParticleTrack G400 probes in a range of
`standard laboratory glass joints on round-bottomed flasks or jacketed lab reactors.
`
`All installation requirements should be discussed with your METTLER TOLEDO Technology
`and Applications Consultant.
`
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`8 Operating Instructions
`During system installation, a trained METTLER TOLEDO engineer makes all system
`connections and verifies the system is ready for use.
`
`1.
`
`If applicable, attach the correct interchangeable probe tip. If interchangeable tips have
`been configured for the given probe and a larger (or smaller) probe diameter would
`be better suited to the current particle system vessel, change the probe tip. Refer to
`the quick reference guide for further details--- “QuickRef-Changing ParticleTrack G400
`Interchangeable Tips" (MK-PB-080-AC).
`
`2. If required, start the pre-purge.
`
`3. Press the Power button on the front of the ParticleTrack G400 base unit and verify the
`Power On indicator illuminates.
`
`4. Allow 30 minutes for the instrument electronics to warm up before taking critical
`measurements.
`
`5.
`
` Turn on the computer and start the iC FBRM software. To connect/configure the
`instrument in iC FBRM, please refer to the applicable software user guide.
`
`6. For dual system configuration, repeat steps 1 through 5 for second
`ParticleTrack G400 system.
`
`7. Observe the indicator LEDs on the front of the ParticleTrack G400 for an indication of
`the system status.
`
`Status
`
`System is powered.
`System is communicating with the FBRM service.
`Computer is off, FBRM service is off, or system needs to be
`connected in iC FBRM.
`HARDWARE STATUS—Hardware error exists that results in
`loss of particle/droplet measurements. Check iC FBRM
`Events Viewer for detailed description.
`Normal status
`SOFTWARE STATUS—Software issue error occurs for
`calculating Chord Length Distribution (CLD) that may
`cause loss of measurement. Check iC FBRM Events Viewer.
`Normal status
`
`Indicators
`
`Power
`
`Color
`
`LED
`State
`Green ON
`ON
`OFF
`
`Communication Green
`
`HW Status
`
`Red
`
`SW Status
`
`Red
`
`ON
`
`OFF
`ON
`
`OFF
`
`Table 7. ParticleTrack G400 LEDs
`
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`9 Best Practices for Routine Operation
`
`Ensure Reliable Instrument Performance
`
`• Follow recommended calibration validation procedures monthly or quarterly
`as determined by your SOP.
`
`• Follow preventative maintenance guidelines for your ParticleTrack instrument.
`
`• Check probe window cleanliness as part of routine SOP.
`
`Ensure Measurement Sensitivity by Optimizing Probe Location and
`Positioning
`
`• Probe should be positioned in the process where it can obtain maximum
`sensitivity to changes in particle or droplet system.
`
`• Probe must be oriented to ensure particle system flows optimally across the
`probe window surface.
`
`• Probe tip must remain fully immersed to provide measurements of the
`particle/droplet system.
`
` -
` -
` -
`
`• Probe location is more critical under the following conditions:
` -
`Extreme difference between particle density compared to the carrying
`solution density (ranges from very low or very high).
`Lower Rheology
`Larger median particle dimension
`Greater deviation between average particle shape and a sphere (more
`irregular particles or particle structures).
`• Probe location is less critical under the following conditions:
` -
`Smaller difference between particle density compared to carrying
`solution density.
`Higher solids concentration (or higher dispersed phase in liquids)
`Smaller median particle dimension.
`Narrower particle distribution.
`Smaller deviation between average particle shape and a sphere (fewer
`irregular particles or particle structures)
`
` -
` -
` -
` -
`
`Track Particle Systems Reliably
`• Use iC FBRM as the reliable SOP for routine monitoring of particle and droplet
`systems in the laboratory.
`
`• Use iC FBRM for advanced data analysis of collected data.
`
`• Use iC FBRM for further improvement and optimization of templates to be
`used in application-specific SOPs.
`
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`Develop a Standard Operating Procedure (SOP)
`• Select or create an appropriate iC FBRM template for each given application. A well-
`designed template will simplify the startup procedure and ensure consistent operation
`in each experiment.
`
`•
`
`•
`
`Include appropriate statistical trends that can directly track particle and product
`quality parameters of interest.
`
`Include reference and target distributions as process milestones or final product
`quality set-points.
`
`• Optimize the measurement configuration (measurement interval and averaging
`settings) to ensure robust repeatable measurement and to maximize sensitivity to
`dynamic changes in the particle system.
`
`Save Experiment Settings as a Template—Make sure to select the right template for
`a specific particle or droplet system. Use a template that includes trends and reference
`distributions that are important to track in order to characterize the particle or droplet
`system.
`
`Manage Reference Distributions—Distributions can be saved as references and
`designated as targets for subsequent experiments. Reference distributions or target
`distributions can be saved in particle-specific templates.
`
`Check Probe Window Cleanliness—The probe window must be clean before mounting
`in particle or droplet system and before performing Calibration Validation.
`
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`10 Troubleshooting
`Errors are generally hardware-related issues that affect data acquisition. The following
`table documents how hardware errors are displayed in the control software, describes
`what the error means, and provides possible root causes to assist with troubleshooting
`and resolving the issue. If the issue cannot be resolved, please contact the AutoChem
`Market Support Group for assistance.
`
`Errors
`Error Message
`Box temperature
`high / low
`
`Scan speed or
`Scan frequency
`high / low
`
`Tach Pulse missing
`Note: SW Status LED
`illuminates red for
`this error if it persists.
`
`Description
`Internal temperature of base
`unit has fallen outside of the
`operating temperature range
`(5 °C to 35 °C).
`Desired scan speed or
`frequency is outside
`acceptable range.
`
`Data acquisition error.
`
`Possible Cause
`The base unit is installed in a
`location that is not within
`recommended specification.
`
`Bearings nearing end of life or
`incorrect probe configuration. Check
`configuration. If error continues,
`contact METTLER TOLEDO.
`Verify USB connections are secure. If
`error continues, contact
`METTLER TOLEDO.
`
`Table 8. Troubleshooting errors
`
`Warnings
`Warning Message
`
`ProbeA Effective
`Duration Low
`Note: SW Status LED
`illuminates red for
`this warning if it
`persists.
`
`Average Signal
`Intensity High
`
`Average Signal Intensity is an
`indicator of the amount of
`light backscattered by the
`particles or droplets being
`measured.
`
`Table 9. Troubleshooting warnings
`
`Description
`
`Possible Cause
`
`Effective Duration reports the
`percentage of the scan signal
`from the previous measure-
`ment interval used to
`calculate the currently
`displayed Chord Length
`Distribution (CLD). Normal
`operation results in an
`Effective Duration of
`approximately 50%.
`
`Effective Duration Low may indicate
`that the PC specifications are
`inadequate for complete transfer and
`processing of the available signal. A
`low Effective Duration may reduce
`the precision of the measurement.
`If the Effective Duration is
`significantly less than 40%, contact
`METTLER TOLEDO. The
`measurement interval can also
`impact Effective Duration. Only
`select an interval <10 s where you
`expect rapid process changes.
`Average Signal Intensity High may
`indicate that the particles being
`measured are highly reflective. Very
`high backscatter may saturate the
`sensor, resulting in erroneous
`measurements.
`
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`11 Product Maintenance
`METTLER TOLEDO warrants its products against defects in materials and workmanship for
`twelve months from the date of installation or fifteen months from the date of shipment,
`whichever comes first. For details, please refer to the warranty provided with the
`instrument. For assistance, please email AutoChemCustomerCare@mt.com.
`It is recommended that you retain the original packing materials if you need to return
`the ParticleTrack system. If factory service is required, your METTLER TOLEDO service
`engineer will issue you a Return Material Authorization (RMA) form.
`There are no user-serviceable parts inside a ParticleTrack G400. Contact your
`METTLER TOLEDO Field Service Engineer for all service needs.
`
`Schedule the following maintenance tasks:
`
`• Run the Calibration Validation procedure for the probe every three to six months, if the
`probe is dropped or the system is transported, and after new software is installed, if
`desired.
`
`The “Calibration Validation in iC FBRM” procedure uses the PVC Reference Sample and
`reference file, provided with the system. The procedure also requires a Fixed Beaker
`Stand (FBS). Locate the procedure document in the ParticleTrack G400 Hardware
`Portfolio.
`
`• Clean the probe window periodically. To clean the outside window, use a medium
`such as water, alcohol, or acetone to clear the surface. A fine, abrasive polishing
`compound may be used to remove stubborn stains (0.3 micron alumina, used to
`polish optical surfaces is recommended). After cleaning, use a dry, clean Kimwipe®
`to remove the cleaning solution. The probe window cleanliness can be verified in the
`software.
`
`• Ensure the air/gas supply meets the required standards, when using the optional
`purge.
`
`• Change bearings, if necessary, as recommended by METTLER TOLEDO. The average
`life of the bearings on the ParticleTrack G400 is one to two years. Under normal
`operating conditions, the probes should be serviced every other year during Preventive
`Maintenance to ensure optimal uptime with no unexpected failures. Probes operated
`at elevated temperatures and/or continuously must be serviced more frequently, and
`in this case a Full Coverage Service Contract is recommended. To extend bearing life,
`turn off the probe when not in use.
`
`• The ParticleTrack G400 system is designed for indoor use, so the base unit and probe
`back end can only be wiped clean. The wetted portion of the probe tip can be cleaned
`with solvent such as ethanol, IPA, or soap and water.
`
`METTLER TOLEDO has offices around the world. Contact the Mettler-Toledo AutoChem,
`Inc., headquarters in the USA for technical support or service. To arrange for specific
`application assistance from a METTLER TOLEDO Technology and Applications Consultant,
`or for assistance, contact Customer Care through the toll-free number on page 2.
`
`16
`
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`
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`
`Recommended Maintenance
`
`A qualified METTLER TOLEDO Field Service Engineer should perform regular Preventive
`Maintenance (PM) on the system. Table 10 shows the normal life expectancy of several
`component parts and identifies any customer-replaceable parts. Use this information for
`planning potential cost of ownership.
`
`Replacement Interval
`Annually
`
`Every two (2) years
`Every three (3) years
`
`Table 10. Parts life expectancy
`
`Part
`
`PVC Reference Sample, G400
`• customer-replaceable
`• PVC life: 10 uses or one year, whichever comes first
`• included in annual PM.
`Scanning assembly
`Laser Board
`
` Relocation, Shipment, or Storage
`To prevent and minimize damage to the ParticleTrack G400, follow the instructions below
`to prepare the system for relocation, shipment, or storage.
`
`1. Close the iC FBRM software application and shutdown the computer according to
`normal operating procedures.
`
`2. Disconnect the power, air, and communications from the back panel of the base unit.
`
`3. Disconnect the USB cable from the control computer.
`
`4. Store the system and all components in the factory-supplied box.
`
`12 Disposal
`
`
`Please dispose of this product in accordance with local regulations at the collecting point
`specified for electrical and electronic equipment.
`If you have any questions please contact the responsible authority or the distributor from
`which you purchased this device.
`Thank you for your contribution to environmental protection.
`
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`
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`
`Our on-demand webinars (online seminars) provide application
`and industry information relevant to you. These interactive
`presentations, provided by industry experts and our own
`applications team, give you an opportunity to learn more about
`your specific area of interest.
`
`Topics include:
`•
`Improving Crystallization and Precipitation Processes
`•
`The Importance of Mixing in Process Development
`•
`Avoiding Incidents During Scale-up
`•
`Recent Advances in Organic Chemistry
`•
`Calorimetry Best Practices
`•
`Characterization of Catalytic Hydrogenations
`•
`Plus other applications including green chemistry, organic
`synthesis, fermentation, high pressure chemistry and more
`
` www.mt.com/ac-webinars
`
`www.mt.com/ParticleTrack
`
`Visit for more information
`
`Mettler-Toledo AutoChem, Inc.
`7075 Samuel Morse Drive
`Columbia, MD 21046 USA
`Telephone +1 410 910 8500
`Fax +1 410 910 8600
`
`Email autochem@mt.com
`Internet www.mt.com/autochem
`
`Subject to technical changes
`© 4/2016 Mettler-Toledo AutoChem, Inc.
`Printed in USA MK-PB-0065-AC Rev F DCN 2872
`
`Learn More with our
`Technical Webinar Program
`
`