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`Merck Exhibit 2144, Page 1
`Mylan v. Merck, IPR2020-00040
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`Merck Exhibit 2144, Page 2
`Mylan v. Merck, |PR2020-00040
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`Merck Exhibit 2144, Page 2
`Mylan v. Merck, IPR2020-00040
`
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`Merck Exhibit 2144, Page 3
`Mylan v. Merck, |PR2020-00040
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`Merck Exhibit 2144, Page 3
`Mylan v. Merck, IPR2020-00040
`
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`Merck Exhibit 2144, Page 4
`Mylan v. Merck, |PR2020-00040
`
`Merck Exhibit 2144, Page 4
`Mylan v. Merck, IPR2020-00040
`
`
`
`File Name
`
`Experiment
`Operator
`Experiment ID
`Sample Name
`~ Sample Lot #
`Notes
`
`Drying Temp
`Heating Rate
`Max Drying Time
`Equil Crit
`Expt Temp
`Max Equil Time
`Equil Crit
`RH Steps
`Data Logging Interval
`Expt Started
`Run Started
`
`Elap Time
`min
`
`71.1
`81.7
`96.6
`105.6
`115.4
`126.1
`137.1
`148.1
`159.1
`170.1
`181.1
`192.4
`203.1
`229.5
`284.8
`327.1
`374.7
`464.6
`585.3
`771.1
`957.1
`1060.2
`1105.8
`1137.9
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`1183.8
`1203.7
`1220.9
`1237.1
`1252.7
`1267.4
`1282.8
`1307.1
`1329.2
`1345.9
`1364.7
`1383.3
`1394.4
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`Weight
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`8.268
`8.270
`8.273
`8.275
`8.277
`8.280
`8.283
`8.286
`8.289
`8.292
`8.295
`8.299
`8.308
`8.321
`8.612
`8.682
`8.775
`8.952
`9.290
`10.334
`9.383
`8.975
`8.799
`8.698
`8.626
`8.576
`8.533
`8.498
`8.465
`8.436
`8.410
`8.386
`8.366
`8.343
`8.326
`8.311
`8.302
`8.298
`
`26180132.!sh
`
`Step Isotherm
`LS
`261801 32
`L-000221869
`
`phosphate salt lot 70316-153
`DP-IV
`N826180-132
`40 °C
`5 °Clmin
`60 min
`0.0100 wt % in
`25 °C
`180 min
`0.0100 wt % in
`
`5 to 95 to 5 in 5% RH steps
`2.00 min or
`09/16/2002
`16:49:40
`
`Weight
`% chg
`0.000
`0.020
`0.054
`0.077
`0.107
`0.146
`0.179
`0.213
`0.248
`0.284
`0.322
`0.375
`0.484
`0.644
`4.162
`4.999
`6.129
`8.267
`
`Samp Temp
`deg C
`25.49
`25.33
`25.30
`25.30
`25.29
`25.28
`25.27
`25.27
`25.26
`25.26
`25.26
`25.26
`25.26
`25.26
`25.25
`25.25
`25.25
`25.25
`
`12.361
`24.988
`13.477
`8.542
`6.424
`5.201
`4.322
`3.719
`3.198
`2.775
`2.375
`2.032
`1.715
`1.422
`1.180
`0.907
`0.695
`0.518
`0.407
`0.364
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`25.24
`25.24
`25.24
`25.25
`25.25
`25.25
`25.25
`25.25
`25.25
`25.25
`25.25
`25.25
`25.25
`25.25
`25.25
`25.25
`25.25
`25.25
`25.25
`25.25
`
`2.00 min
`
`5.00 min
`
`0.0100 wt %
`
`RH
`
`Samp
`%
`
`1.96
`5.10
`10.06
`15.06
`19.88
`24.87
`29.78
`34.88
`39.84
`44.89
`49.87
`54.93
`59.97
`64.89
`69.85
`74.87
`79.89
`85.02
`89.70
`94.70
`90.01
`85.32
`80.27
`75.34
`70.09
`65.14
`60.00
`55.08
`50.16
`45.10
`40.09
`35.03
`29.96
`24.97
`‘ 20.17
`15.22
`10.22
`4.78
`
`Merck Exhibit 2144, Page 5
`Mylan v. Merck, |PR2020-00040
`
`Merck Exhibit 2144, Page 5
`Mylan v. Merck, IPR2020-00040
`
`
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`Merck Exhibit 2144, Page 6
`Mylan v. Merck, IPR2020-00040
`
`
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