`
`
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`
`
`Merck Exhibit 2130, Page 1
`Mylan v. Merck, |PR2020-00040
`
`Merck Exhibit 2130, Page 1
`Mylan v. Merck, IPR2020-00040
`
`

`

`MERCK & CO., INC.
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`NOTEBOOK PROCEDURE*
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`October, 1999
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`,
`
`Merck Exhibit 2130, Page 2
`Mylan v. Merck, |PR2020-00040
`
`Merck Exhibit 2130, Page 2
`Mylan v. Merck, IPR2020-00040
`
`

`

`
`
`NOTEBOOK NUMBER: 72 7
`q /
`
`A0
`
`AsmGNEDTO:
`c
`t” r B H,
`Print
`
`Signature (/féfLL/x
`
`DATE:
`
`.903
`'6
`
`
`'
`
`':
`11
`
`§
`’v
`
`MERCK
`
`Merck & (30., Inc.
`
`LABORATORY NOTEBOOK
`
`Merck Exhibit 2130, Page 3
`Mylan v. Merck, |PR2020-00040
`
`Merck Exhibit 2130, Page 3
`Mylan v. Merck, IPR2020-00040
`
`

`

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`Merck Exhibit 2130, Page 4
`Mylan v. Merck, IPR2020-00040
`
`

`

`erck Exhibit 2130, Page 5
`v. Merck, |PR2020-00040
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`Merck Exhibit 2130, Page 5
`Mylan v. Merck, IPR2020-00040
`
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`Merck Exhibit 2130, Page 6
`Mylan v. Merck, IPR2020-00040
`
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`erck Exhibit 2130, Page 7
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`Merck Exhibit 2130, Page 7
`Mylan v. Merck, IPR2020-00040
`
`

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`Merck Exhibit 2130, Page 8
`Mylan v. Merck, IPR2020-00040
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`Merck Exhibit 2130, Page 9
`Mylan v. Merck, IPR2020-00040
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`Mylan v. Merck, IPR2020-00040
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`Merck Exhibit 2130, Page 11
`Mylan v. Merck, IPR2020-00040
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`Mylan v. Merck, IPR2020-00040
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`erck Exhibit 2130, Page 13
`v. Merck, |PR2020-00040
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`Merck Exhibit 2130, Page 13
`Mylan v. Merck, IPR2020-00040
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`Merck Exhibit 2130, Page 14
`Mylan v. Merck, IPR2020-00040
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`v. Merck, |PR2020-00040
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`Merck Exhibit 2130, Page 15
`Mylan v. Merck, IPR2020-00040
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`Merck Exhibit 2130, Page 16
`Mylan v. Merck, IPR2020-00040
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`v. Merck, |PR2020-00040
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`Merck Exhibit 2130, Page 17
`Mylan v. Merck, IPR2020-00040
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`Merck Exhibit 2130, Page 18
`Mylan v. Merck, IPR2020-00040
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`erck Exhibit 2130, Page 19
`v. Merck, IPR2020-00040
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`Merck Exhibit 2130, Page 19
`Mylan v. Merck, IPR2020-00040
`
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`Merck Exhibit 2130, Page 20
`Mylan v. Merck, IPR2020-00040
`
`

`

`
`
`28
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`" erck Exhibit 2130, Page 21
`v. Merck, |PR2020-00040
`
`Merck Exhibit 2130, Page 21
`Mylan v. Merck, IPR2020-00040
`
`

`

`Current Data Parameters
`NAME
`MK-431
`EXPNO
`1
`PROCNO
`1
`
`F2 - Acquisition Parameters
`Date_
`20041216
`Time
`8.25
`INSTRUM
`spect
`PROBHD
`5 mm QNP
`1H
`PULPROG
`2930
`TD
`32768
`SOLVENT
`CDC13
`NS
`32
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`6578.947 Hz
`FIDRES
`0.200774 Hz
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`2.4904180 sec
`RG
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`76.000 usec
`DE
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`0.10000000 sec
`
`:::::::::::: CHANNEL fl :::::::::::::
`NUCl
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`399.8724592 MMz
`
`F2 - Processing parameters
`SI
`16384
`SF
`399.8700207 MHZ
`WDW
`no
`8813
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`1.40
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`1D NMR plot parameters
`CX
`40.00 cm
`FlP
`9.750 ppm
`F1
`3898.73 Hz
`F2P
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`F2
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`0.25000 ppm/cm
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`99.96751 Hz/cm
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`
`Merck Exhibit 2130, Page 22
`Mylan v. Merck, |PR2020—00040
`
`Merck Exhibit 2130, Page 22
`Mylan v. Merck, IPR2020-00040
`
`

`

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`Merck Exhibit 2130, Page 23
`Mylan v. Merck, |PR2020-00040
`
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`Merck Exhibit 2130, Page 23
`Mylan v. Merck, IPR2020-00040
`
`

`

`/w/data/hansen/nmr/lactam/l/pdata/l/screen
`
`Thu Dec 16 08:20:18 2004
`
`ooqmmpwwb—I
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`Merck Exhibit 2130, Page 24
`Mylan v. Merck, |PR2020—00040
`
`Merck Exhibit 2130, Page 24
`Mylan v. Merck, IPR2020-00040
`
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`Merck Exhibit 2130, Page 25
`Mylan v. Merck, |PR2020-00040
`
`Merck Exhibit 2130, Page 25
`Mylan v. Merck, IPR2020-00040
`
`

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