throbber
WO 98/03265
`
` PCT/JP97/02472
`
`1
`
`Specification
`
`A cap-shaped reagent vessel for analysis reagents
`
`[Technical Field]
`The present invention relates to a cap-shaped reagent vessel for analysis reagents by which water quality
`analysis is simply performed.
`
`[Background Art]
`Many of analysis methods of an easy water quality analysis adopt a colorimetric analysis.
`As to the colorimetric analysis, since the characteristics are such that devices used are small and
`light, and also low priced, and the result can be seen visually as colors, and the measurement result is fast
`etc., colorimetric analysis is widely used in industry. However, in such colorimetric analysis, since
`chemical agents are used, it requires chemical knowledge, techniques, experience, etc.
`Moreover, since many types of chemical agents are used, not only more than a few types of
`reagents are required to be prepared, but also, and its storage is required. Further, in order to use reagents,
`weight meters such as scales, measuring cylinders etc. and capacity measuring instruments are necessary
`to fractionate required amounts to use reagents, and many beakers and flasks are necessary to churn and
`store them.
`Because of this, if one wants to perform on site water quality analysis, fractionation work of
`reagents etc. are very difficult, but also, depending on the situation, water quality analysis is not possible.
`As to the reagents for water quality analysis, there are liquid forms and powder forms. As to
`liquid reagents, there are different methods in which the reagent stored in glass bottles and plastic bottles
`is fractionated by an accompanying dropper, or fractionated by the dropper built into the glass or plastic
`bottles, or dripped by eye droppers.
`
`(SUBSTITUTE) ANCESTRY EX. 1011
`
`1
`
`

`
`WO 98/03265 PCT/JP97/02472
`
`2
`
` On the other hand, as to powder reagents, there are some methods in which the reagent stored in
`glass or plastic vessels is fractionized by an accompanying light weight spoon, or depending on the case,
`as to the reagent that are packed into a bag with laminated packaging one at a time, or packed into soft
`plastic tube with both ends welded, the packaging is cut and the reagent is added to test water etc. Further,
`liquid or powder reagent is sometimes pre-sealed one at a time into the colorimetic cells made of
`transparent glass and transparent plastic.
`Furthermore, liquid or powder reagent is pre-sealed one time portion at a time into the
`coloriometic cell itself made of transparent glass and transparent plastics.
`By the way, if more than two types of liquid or powder reagents that cannot be mixed and stored
`are used, it is necessary to repackage and store each of them; if test water analysis is performed, each
`reagent must be inputted into the test water separately according to the use method. Hence, more the
`number of reagents, more complicated the analysis work, and if the handling method is different by each
`reagent, the user can get mixed up.
`On the other hand, one can think of inputting the reagent automatically by machines etc., and
`performing automatic measurements, but if there are many inputting reagents, the structure gets
`complicated, and also reagent storage methods are complicated in like fashion as above.
`By the way, there are some methods that were worked on storing the reagent that could not be
`mixed and stored separately, and mixing them simply when used. That is, this is not the purpose for
`handling reagents for analysis but for instance, glass ampule tightly sealed with liquid reagent is placed
`into the soft plastic tube with other reagents, and when in use, an impact is applied on the soft plastic to
`break the glass ampule inside to mix the reagents. Moreover, a method exists in which the substance that
`cannot be mixed and stored are placed into double bags separately and when used, a pressure is applied
`from outside, and the only bag insides is broke.
`
`2
`
`

`
`WO 98/03265
`
` PCT/JP97/02472
`
`3
`
` However, using such an operation method, it not only needs deliberate operations but also the
`operation method could be different for each use purpose, so the user gets confused about the operation
`procedures and methods.
`As described above, in performing the easy water quality analysis, in using the above colorimetric
`analysis, some characteristics were that the devices to be used were small and light and also low priced,
`and the result could be visually seen as colors and measurement result was fast, but due to the reasons that
`preparation and storage of reagent to be used and handling of the reagent were troublesome etc., the flaw
`was that it needed the sufficient chemical knowledge and experience etc. to analyze water quality.
`
`[Disclosure of the invention]
` The first technical challenge of the present invention is to provide a cap-shaped reagent vessel for
`analysis reagents that can perform safe and accurate water quality analysis by a simple operation even
`without chemical knowledge.
` The second technical challenge of the present invention is to simplify the production processes.
`The solution method of the first technical challenge of the present invention comprises, as written in the
`scope 1 of the claims, a transparent vessel main body which enables inputting the test water of a specified
`amount from the opening; a lid body which can be mounted from the aforementioned opening unit side
`of the vessel main body; a reagent storage vessel which houses a specified reagent; a cutter which is
`pushed into the aforementioned lid body, depending on mounting amount of the aforementioned lid body
`with respect to the aforementioned vessel main body, and breaks through the aforementioned reagent
`storage vessel loaded into the aforementioned lid body so that the aforementioned reagent is discharged
`into the aforementioned vessel main body.
` According to this solution method, after inputting a test water of a specified amount into the
`transparent vessel main body, when the lid body which holds the reagent storage vessel housed with a
`specified reagent is mounted from the opening of the vessel main body inside thereof, the cutter is moved
`depending on the tightening amount, and the reagent storage vessel is broken through thus, the reagent
`inside the reagent storage vessel is discharged into the vessel main body.
`
`3
`
`

`
`WO 98/03265
`
` PCT/JP97/02472
`
`4
`
` Hence, when test water is analyzed, the lid body is tightened into the vessel main body with test water
`inputted, thereby, the reagent can be mixed into the test water, hence even with no chemical knowledge,
`safe and accurate water quality analysis is performed by a simple operation.
` Moreover, other solution method of the first technical challenge of the present invention is that as
`described in the scope 2 of the claims, the aforementioned lid body is mounted by tightening from the
`aforementioned opening side of the aforementioned vessel main body, and the aforementioned cutter is
`pushed into the aforementioned lid body depending on the tightening amount of the aforementioned lid
`body with respect to the aforementioned vessel main body.
` According to the solution method, depending on the tightening amount of the lid body with respect to
`the vessel main body, the cutter is pushed into the lid body; hence this has the same effects as the scope 1
`of the claims.
` Moreover, according to the other solution method of the first technical challenge of the present
`invention, as described in the scope 3 of the claims, the aforementioned lid body is mounted by being
`pushed in from the aforementioned opening side of the aforementioned vessel main body, and the
`aforementioned cutter is pushed into the aforementioned lid body depending on the push amount of the
`aforementioned lid body with respect to the aforementioned vessel main body.
` According to the solution method, since the cutter is pushed into the lid body depending on the
`amount of push of the lid body with respect to the vessel main body, this has the same effects as the scope
`1 of the claims.
` Moreover, according to the other solution method of the first technical challenge of the present
`invention, as described in the scope 4 of the claims, a plural number of reagent storage vessels which
`store mutually different reagents is housed inside the aforementioned lid body along the moving direction
`of the aforementioned cutter, so depending on the mounting, tightening and push of the aforementioned
`lid body, the aforementioned plural number reagent storage vessels are broken thru sequentially by the
`aforementioned cutter.
` According to this solution method, a plural number of reagent storage vessels are housed on the lid
`body along the moving direction of the cutter and when handling the reagent storage vessel of analysis
`reagent with the test water,
`
`4
`
`

`
`WO 98/03265
`
` PCT/JP97/02472
`
`5
`
`The lid body is mounted, tightened or pushed to the vessel main body with test water inputted, thus each
`reagent is mixed with test water sequentially.
` Moreover, according to the other solution method of the first technical challenge of the present
`invention, as described in the scope 5 of the claims, a packing was mounted on the lower surface side of
`the aforementioned cutter, and due to the mounting, tightening or push of the aforementioned lid body
`with respect to the aforementioned vessel main body, the opening edge part of the aforementioned vessel
`main body abuts the aforementioned packing, and the aforementioned vessel main body and the
`aforementioned lid body inside are tightly sealed.
` According to the solution method, due to the tightening of the lid body, the packing mounted on the
`lower surface side of the cutter abuts the opening edge part of the vessel main body, thereby, the vessel
`main body and the lid body inside are tightly sealed, hence even when test water and reagent are churched,
`these test water and reagent do not leak outside.
` Moreover, according to the other solution method of the first technical challenge of the present
`invention, as described in the scope 6 of the claims, a soft material protector is intervened between the
`aforementioned reagent storage vessel and the aforementioned cutter, thus the aforementioned reagent
`storage vessel is protected so that it is not damaged carelessly by the aforementioned cutter.
` According to this solution method, due to the protector of a soft material held between the reagent
`storage vessel and the cutter, the contact of the reagent storage vessel and the cutter is designed to be
`interrupted, so when test water is not analyzed, the reagent storage vessel is not broken through by a
`cutter by mistake, thus the reagent storage vessel is surely saved.
` According to the other solution method of the first technical challenge of the present invention, as
`described in the scope 7 of the claims, a spacer to promote the movement halt of the aforementioned
`cutter accompanied by mounting, tightening and pushing-in of the aforementioned lid body is intervened
`between aforementioned reagent storage vessels, hence a moderation is provided for breaking thru of the
`aforementioned reagent storage vessels by the aforementioned cutter.
` According to the solution method, a spacer is intervened between reagent storage vessels, to provide
`moderation for breaking thru of the aforementioned reagent storage vessels by the aforementioned cutter,
`hence
`
`5
`
`

`
`WO 98/03265
`
` PCT/JP97/02472
`
`6
`
`When time differences, etc. is necessary for inputting reagents, tightening of the lid body can be adjusted
`by a sense of moderation.
`According to the other solution method of the first technical challenge of the present invention, as
`described in the scope 8 of the claims, the aforementioned cutter comprises a disk-shaped cutter bottom
`part with a plural number of reagent passage holes; a plural number of slits which protrude in the center
`of the cutter bottom part, and is enabled to communicate with the aforementioned reagent passage hole on
`the side surface; and also, crescent moon-shaped cutter blade edge at the front end.
` According to the solution method, the reagent inside the reagent storage vessel broken thru by cutter
`blade edge leaks out to the outside of reagent storage vessel along the plural number of slits formed on the
`side surface of the cutter cylinder part, and by collapsing and churning the vessel main body in this
`condition, the test water and reagent inside the vessel main body get mixed up via the plural number of
`reagent passage holes at the cutter bottom part.
` According to the other solution method of the second technical challenge of the present invention, as
`described in the scope 9 of the claims, the aforementioned cutter comprises: a disk-shaped cutter bottom
`part; a crown-shaped cutter blade edge formed by raise by cuts at the center of the cutter bottom part;
`reagent passage hole formed in the center.
` According to the solution method, since the cutter blade edge is cut and raised in the center of the
`cutter bottom part, and at the same time, reagent passage holes are formed, the production process is
`simplified.
` According to the other solution method of the second technical challenge of the present invention, as
`described in the scope 10 of the claims, the aforementioned cutter blade edge comprises the plural number
`of blade pieces where the center of the cutter bottom was cut and raised.
` According to this solution method, the cutter blade edge is formed by cutting and raising the center
`part of the cutter bottom part, and in the same time, reagent passage holes are formed, hence this plays the
`same effects as those in the scope 9 of the claims.
`
`6
`
`

`
`WO 98/03265
`
` PCT/JP97/02472
`
`7
`
` Moreover, according to the other solution method of the second technical challenge of the present
`invention, as described in the scope 11 of the claims, bending - processed flange unit is provided at the
`periphery edge part of the aforementioned cutter bottom part.
` According to the solution method, by providing a bending processed flange part at the periphery edge
`of the cutter bottom, rigidity of the cutter bottom part was enhanced, this enabled the plate thickness of
`the cutter bottom part to be thinner, and thus cost reduction was attempted along with simplification of
`production process.
` [Brief explanation of drawing]
`Fig. 1 is a cross section drawing showing an embodiment of the cap-shaped reagent vessel for analysis
`reagents of the present invention. Fig. 2 is a perspective drawing showing a protector of Fig. 1. Fig. 3 is a
`perspective drawing showing the cutter of Fig. 1. Fig. 4 is a cross section showing other embodiment
`when the cutter configuration in Fig. 1 is changed. Fig. 5 is a perspective drawing showing the cutter in
`Fig. 4. Fig. 6 is a cross section showing the cutter in Fig. 4. Fig. 7 is a perspective drawing showing other
`embodiment when the configuration of the reagent storage vessel of the analysis reagent in Fig. 1 is
`changed.
`[Best main body of the invention]
`The following explains the detail of the embodiment of the present invention based on the drawings.
`Fig. 1 thru Fig. 3 shows one embodiment of the cap-shaped reagent vessel for analysis reagents of the
`present invention.
` As shown in these drawings, as to the reagent vessel, as the female screw part 2 of the cap body 3 is
`screwed into screw 19 of transparent vessel main body 15 to be colorimetric cells, the cap body 3 is free
`to be fitted into the vessel main body 15.
` In the internal center of the cap body 3, a groove 1 is formed into which the crescent moon-shaped
`cutter blade edge 9 of the cutter 8A later mentioned which is pushed up by screwing the cap body 3 is
`fitted.
`
`7
`
`

`
`WO 98/03265 PCT/JP97/02472
`
`8
`
` Inside the cap body 3 are housed chemical resistant film vessels 4 and 5 which house different types
`of reagents. Moreover, as to the housing state of these film vessels 4 and 5, it is designed to be along the
`moving direction of cutter 8A.
` Here, as to each film vessels 4 and 5 it is good if they have high barrier resistance (moisture, acid) and
`high chemical resistance, and this comprises multi-layered/ composite structure laminated packaging
`material.
` Specifically, from the outside in order, there is a 4-layer structure of polyester (12 µ) – polyethylene
`(15 µ) – aluminum (7 µ) – polyethylene (25 µ).
` Further, polypropylene and PET etc. can be used.
` In the lower part of the film vessel 5 is provided a protector 7 made of soft material such as paper and
`hard plastic cutter 8A.
` The protector 7 is used to prevent careless breaking of film vessel 4, 5 by a cutter 8A, and as shown in
`Fig. 2, it is configured such that in the center of disk-shaped protector body 7a, protector hole 13 is
`formed and also, a bent piece 18 is provided in the periphery edge part of the protector main body 7a.
`Then, as described later, when the cutter 8A pushes up the protector main body 7a, the protector main
`body 7a is designed to be bent from the crease 18a of the bent piece 18.
` The cutter 8A, as shown in Fig. 3, comprises a disk-shaped cutter bottom part 8a. On the cutter bottom
`part 8a, a plural number of reagent passage holes 10 are provided, and is designed so that reagent inside
`film vessels 4 and 5 and test water inside vessel main body 15, while moving through these reagent
`passage holes 10, get mixed up.
` Moreover, on the lower surface side of cutter bottom part 8a, a doughnut-shaped packing 11 is
`provided that comprises a plural number of protrusions 12 and whose diameter is somewhat larger than
`cutter bottom part 8a.
`
`8
`
`

`
`WO 98/03265 PCT/JP97/02472
`
`9
`
`Then, it is designed such that when the cutter 8A is housed into the cap body 3, as the protrusion 12 of the
`packing 11 thrusts into the cap body 3, falling out of cutter 8A are prevented. Further, the center part of
`the cutter bottom part 8a has a crescent moon-shaped cutter blade 9 at the front edge, and also on the side
`is provided a cutter tube 8 with a plural number of slits 14.
` On the other hand, a scale 16 is formed on transparent vessel main body 15, and designed to be the
`standard position of the amount of test water to be taken into the vessel main body 15. Moreover, opening
`edge part of the screw 19 of vessel main body 15 is designed to be a pedestal 17 of the above described
`packing 11, and when the pedestal 17 abuts the lower surface side of the packing 11 by tightening the cap
`body 3, the space between pedestal 17 and packing 11 is tightly sealed, liquid is prevented from leaking
`outside of the vessel main body 15.
` Following this, the analysis method by the cap-shaped reagent vessel for analysis reagents with such
`configuration is explained. Moreover, in the following analysis method, a case of detecting phosphoric
`3-) of test water is explained.
`acid (PO4
` That is, the test water is poured up to the position of scale 16 of the vessel main body 15 to be a
`colorimetric cell. In this case the amount of test water is about 25 ml.
` In this condition, the vessel main body 15 is put into the cell box of a photoelectric photometer not
`shown in Fig. that detects the concentration of test water by a specified wave length light, and zero
`adjustment of photoelectric photo meter is done.
` Next, vessel main body 15 is taken out from the photoelectric photo meter, and a cap body 3 is
`mounted to the screw 19 of vessel main body 15. At this time, in the film vessel 4 of cap body 3 is stored
`powder reagents that contain ascorbic acid and 10% diluted sulfuric acid that contains ammonium
`molybdate.
`Then when the cap body 3 is tightened while the female screw part 2 of the cap body 3 engages the screw
`19 of vessel main body 15,
`
`9
`
`

`
`WO 98/03265 PCT/JP97/02472
`
`10
`
`First while the pedestal 17 of opening edge part of screw 19 of vessel main body 15 is abutting on the
`lower surface side of packing 1, the cutter 8A is pushed into the cap body 3. Accompanied by this, the
`bent pieces 18 of the protector main body 7a is bent from the crease 18a part accompanied with the
`movement of cutter 8A.
` When the cap body 3 is tightened further from this condition, a crescent moon-shaped cutter blade
`edge 9 of the cutter 8A breaks thru the film vessel 5. Thereby, 10% diluted sulfuric acid that contains
`ammonium molybdate housed inside the film vessel 5 leaks out outside of film vessel 5 along the plural
`number of slits 14 formed on the side of cutter tube 8 of the cutter 8A.
` If the cap body 3 is further tightened from this condition, the cutter blade edge 9 of the cutter 8A
`breaks through the film vessel 4. Thereby, powder reagent that contains ascorbic acid leaks from film
`vessel 4. If the cap body 3 is further tightened from this condition, the crescent moon-shaped cutter blade
`edge 9 of the cutter 8A fits into the groove 1 and the tightening of cap body 3 stops.
` In this condition, if the vessel main body 15 is collapsed and churned, and the reagent is sufficiently
`mixed into the test water, this reacts with PO4
`3- contained in the test water, and this presents the so called
`molybdenum blue color. The reagent is sufficiently mixed with test water, and after leaving it alone for 5
`minutes, vessel main body 15 is set again to the photoelectric photo meter. Thereby, concentration of test
`water is displayed by mg/l.
` Like this, in this embodiment, after specified amount of test water is poured into the transparent vessel
`main body 15, the cap body 3 which holds film vessels 4 and 5 with specified reagent stored is mounted
`by tightening inside from the opening of vessel main body 15, the cutter 8A is moved depending on the
`tightening amount a, and film vessels 4 and 5 are broken thru and the reagent inside film vessels 4 and 5
`is discharged into the vessel main body 15.
`
`10
`
`

`
`WO 98/03265 PCT/JP97/02472
`
`11
`
`Hence, when test water is analyzed, by tightening the cap body 3 into the vessel main body 15 with
`test water poured in, the reagent can be mixed into the test water, hence, without chemical knowledge,
`safe and accurate water quality analysis can be performed using a simple operation.
` Moreover, for one-time analysis of test water, one cap body 3 is fine, and it is not necessary to prepare
`a separate vessel that houses liquid reagent etc.
` Further, since the vessel main body 15 to be colorimetric cells can be shared with respect to all test
`water, the usage can be made as often as you want after washing, and this is very economical.
` Further also, as pedestal 17 abuts the lower surface part of packing 11, this prevent s the liquid from
`leaking outside of the vessel main body 15, so after finishing water quality analysis, even when disposal
`of the liquid or washing of vessel main body 15 and cap body 3 are not possible, one can take them back
`while tightly sealed with lid on.
` Additionally, when the cap-shaped reagent vessel of such analysis reagent is used for an automatic
`measurement device, since the vessel itself has the same shape, the mechanism can be simplified, and also
`it is not necessary to provide the automatic measurement device itself with a storage function of the vessel,
`hence the device can be miniaturized.
` Moreover, in the above embodiment, a case was explained when two pieces of film vessels 4 and 5
`was loaded into the cap body 3, this is not limited to this, and when one film vessel 4 or 5 was loaded, test
`water can be inspected.
` That is, taking an example of nickels measurement, in the same manner as above, test water is input up
`to the scale 16 position of the vessel main body 15 to be colorimetric cells. In this condition, the vessel
`main body 15 is placed into the cell box of the photoelectric photo meter set to the specified wave length,
`the photoelectric photo meter is set to zero adjustment in the same manner as above.
` Next, vessel main body 15 is taken out from the photoelectric photo meter, the cap body 3 which is
`built-in with
`
`11
`
`

`
`WO 98/03265
`
` PCT/JP97/02472
`
`12
`
`reagent showing Ni is mounted to the vessel main body 15 in the same manner as above and lid body 3 is
`tightened. At this time, in the same manner as above, while the pedestal 17 of the opening edge part of
`screw 19 of vessel main body 15 abuts the lower surface side of packing 11, the cutter 8A is pushed into
`eth lid body 3. Accompanied by this, the bent pieces 18 of the protector main body 7a is bent from the
`crease 18a with the movement of cutter 8A.
` When lid body 3 is further tightened from this condition, the crescent-shaped cutter blade edge 9 of the
`cutter 8A break thru film vessels 4, 5 first. Thereby, nickels coloring reagent (powder reagent with
`dimethyl gloyoxime as the main ingredient) housed inside film vessels 4, 5 leaks outside of film vessels 4,
`5 along a plural number of slits 4 formed on the side surface of cutter tube 8 of the cutter 8A. If lid body
`3 is tightened more from this condition, as the crescent-shaped cutter blade edge 9 of the cutter 8A fits
`into the groove 1, tightening of the lid body 3 is stopped.
`At this time, as described, the pedestal 17 of the opening edge part of screw 19 of vessel main body 15
`abuts the lower surface part of packing 11, and between the pedestals 17 and packing 11 is tightly closed,
`thus liquid is prevented from leaking outside of vessel main body 15. In this condition, the vessel main
`body 15 is collapsed and churned, and after the reagent is sufficiently mixed into test water, they are left
`alone for 10 minutes.
` At this time, if the reagent sealed is powder, since it is possible that this can remain in the film vessel 4
`or film vessel 5, churning by collapsing the vessel main body 15 is done sufficiently.
` Then, after 10 minutes, if it is reset to the photoelectric photo meter, concentration can be read by mg/l
`unit.
` Moreover, in this embodiment, a case was explained in which by moving cutter 8A accompanied by
`tightening of lid body 3, the film vessel 4 and/or 5 is designed to be broken thru simply, but this
`embodiment is not limited to this, for instance this can be designed so that a spacer can be intervened
`between the film vessel 4 and 5, moderation can be provided for movement of the cutter 8A.
`
`12
`
`

`
`WO 98/03265
`
` PCT/JP97/02472
`
`13
`
` That is, when more than 2 types of reagents are inputted, sometimes the reaction time of the first
`reagent inputted are needed, and in this case, depending on the moderation feeling of the movement of the
`cutter 8A by spacer, adding and decreasing the tightening the lid main body 3 as a feeling can be known,
`thus anxiety of breaking thru the film vessel 4 and or 5 that houses the next reagents during the previous
`reagent reaction is gone.
` In Fig. 4 thru Fig. 5 are shown the other embodiment when the configuration of the cutter 8A
`described above is changed. Moreover, in the Fig explained in the following, the same symbols are
`added for the parts that are shared with Fig. 1 thru Fig. 3, and duplication explanations are omitted.
` The cutter 20 shown in these figures is made of 0.15mm hard stainless steel. In the center part of the
`cutter bottom part 21 of the cutter 20 is provided a crown shaped cutter blade edge 22. This cutter blade
`22 is made of 4 pieces of blade pieces 23 whose center part of the cutter bottom part 21 is cut and raised
`upward, and inside of these 4 blade pieces 23 is provided reagent passage holes 24 that are formed at
`same time as the raise by cutting.
` In the periphery of the cutter bottom part 21, is provided a flange 25 which is bent downward. It is
`designed such that rigidity of cutter bottom part 21 is enhanced by the flange 25.
` The packing 11 is positioned on the lower surface side of the cutter 20 whose diameter is somewhat
`larger than the cutter bottom part 21, and in its center, communication hole 13 that corresponds with the
`reagent passage holes 24 described above is formed, and in its periphery, protrusion 12 is set up.
` The cap shaped reagent vessel for analysis reagents with such a configuration is used as follows.
` That is, when the lid body 3 is tightened while the female screw part of the lid body 3 is engaged with
`
`13
`
`

`
`WO 98/03265 PCT/JP97/02472
`
`14
`
`the screw part 19 of the vessel main body 15, in the same way as above, while the pedestal 17 of the
`vessel main body 15 abuts the lower surface side of the packing 11, the cutter 20 is pushed into the lid
`body 3. Accompanied by this, the bent piece 18 of the protector main body 7a, along with the movement
`of cutter 8A, gets bent from the crease 18a part.
` When the lid body 3 is further tightened from this condition, the cutter blade 22 of the cutter 20 first
`breaks thru the film vessel 5. At this time, since cutter blade edge 22 comprises 4 pieces of blade pieces
`23, the break thru of the film vessel 5 is easily and surely done.
` By this, 10% diluted phosphoric acid that contains ammonium molybdate housed inside the film vessel
`5 above described moves to the vessel main body 15 sides thru the reagent passage holes 24 formed at the
`center part of the cutter 20.
` When lid body 3 is furthermore tightened form this condition, the cutter blade 22 of the cutter 20
`breaks thru the film vessel 4. At this time, since cutter blade edge 22 comprises 4 blade pieces 23, the
`break thru of the film vessel 5 is easily and surely done.
` By this, powder reagent that contains ascorbic acid leaks from the film vessel 4 described above.
`When the lid body 3 is further tightened from this condition, as the cutter blade 22 of the cutter 20 is fit
`into the groove 1, the tightening of the lid body 3 stops.
` In these conditions, as described above, if vessel main body 15 is collapsed and churned, and reagent is
`3- contained in test water, and this presents a
`sufficiently mixed into test water, it reacts with PO4
`so called molybdenum blue. And reagent is sufficiently mixed into test water and leaving this alone for 5
`minutes, vessel main body 15 is reset to the photoelectric photo meter then, concentration of the test water
`is displayed by mg/l.
`In this manner, in this embodiment, because the tip of the cutter blade 22 is comprised of plural blades 23
`formed by cutting open the central part of the cutter basal means 21, not only is the manufacture thereof
`simple, because there are plural blade tips of the strong blade piece 23, it is easy to perforate through the
`film vessels 4 and 5, in addition to enabling the secure performance thereof.
`
`14
`
`

`
`WO 98/03265 PCT/JP97/02472
`
`15
`
`Moreover, in this embodiment, by providing a flanged means 25 which is fold processed on the outer
`peripheral edge means of the cutter basal means 21, because the brittleness of the cutter basal means 21
`can be increased, the sheet thickness of the cutter basal means 21 can be made thinner in a contrivance at
`simplifying the manufacturing processes thereof as well as reducing the cost thereof.
`Note that in each of the embodiments described above, an explanation was provided of the situation
`where the cutters 8A and 20 are pushed into the interior means of the cap body 3 by means of pressing
`hard the female screw part 2 of the cap body 3 into the biting-in state to the cap body 3 to the screw
`means 19 of the vessel main body 15, not limited to this embodiment, for example, as illustrated in figure
`7, by pressing in the cap body 3 to the vessel main body 15 side, the cutters 8A and 20 can be to be
`pushed into the interior means of the cap body 3.
`That is, a guide protrusion 31 having elasticity is provided on the upper outer periphery of the

This document is available on Docket Alarm but you must sign up to view it.


Or .

Accessing this document will incur an additional charge of $.

After purchase, you can access this document again without charge.

Accept $ Charge
throbber

Still Working On It

This document is taking longer than usual to download. This can happen if we need to contact the court directly to obtain the document and their servers are running slowly.

Give it another minute or two to complete, and then try the refresh button.

throbber

A few More Minutes ... Still Working

It can take up to 5 minutes for us to download a document if the court servers are running slowly.

Thank you for your continued patience.

This document could not be displayed.

We could not find this document within its docket. Please go back to the docket page and check the link. If that does not work, go back to the docket and refresh it to pull the newest information.

Your account does not support viewing this document.

You need a Paid Account to view this document. Click here to change your account type.

Your account does not support viewing this document.

Set your membership status to view this document.

With a Docket Alarm membership, you'll get a whole lot more, including:

  • Up-to-date information for this case.
  • Email alerts whenever there is an update.
  • Full text search for other cases.
  • Get email alerts whenever a new case matches your search.

Become a Member

One Moment Please

The filing “” is large (MB) and is being downloaded.

Please refresh this page in a few minutes to see if the filing has been downloaded. The filing will also be emailed to you when the download completes.

Your document is on its way!

If you do not receive the document in five minutes, contact support at support@docketalarm.com.

Sealed Document

We are unable to display this document, it may be under a court ordered seal.

If you have proper credentials to access the file, you may proceed directly to the court's system using your government issued username and password.


Access Government Site

We are redirecting you
to a mobile optimized page.





Document Unreadable or Corrupt

Refresh this Document
Go to the Docket

We are unable to display this document.

Refresh this Document
Go to the Docket