`E.I. du Pont de Nemours & Co. and
`Acher-Daniels-Midland Co. v. Furanix Technologies BV
`IPR2015-01838
`
`
`
` Experimental
`
`disk I B52955. These cops plenkedjsoold ones "Dig"‘uud.
`gg Add stirring magnet and cap with Avanti
`anual HPHPQCS.
`x Close the blocks according OP-CH-I0 '
`at RT according OP-CH-99: Pressuriscr Work procedure
`5 Bring under pressure with An'_tiIl
`9‘ Plat: in preheated HTHP QCS It LR-041 of , according settings in table 2, mfing
`/I Fill in l0gbocknI'.: HTHPQCS~El3
`4 Place immediately afier the reaction time in an ice bath during 30 minutes.
`
`en and thereb decom ress reactors in a fumehood.
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`gq .-_. i_,,— 197: may
`A ‘x-J3‘! L;:.i:_T"_3.41!.uiv,:f'-1*; ?§’i:~:!«:;:‘Jll.v‘lI‘f.. é”:.-U'(3.‘7 .5
`1 Transfere these dilutions to 7 times to 8 ml vials with Pasteur’s pipettes.
`K Dilute 700 times by 10 in ofdiIutions78 times + 990 pl ofWater in HPLC vials.
`
`
`*.‘:_;‘ ;;r:.:ft~.Tl.“.:'7T.:a ‘-[T‘.<fQ“'.7=.i'!
`
`
`Table 4: Substrate MMF solutions. in table II to 26
`
`SolB HMF/AM]?
`113.34 In ml
`3%
`Acoll ml
`'
`otal V ml
`
`onoentration(mg/ml) O
`Samplespreparedwiththis
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`solution.
`
`0.396
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`i
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`0.263
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`79’’’>;.
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`IIIIIIC
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`ii
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`0xE08l -V49
`XI-3081-V50
`081-V51
`xE08l -V52
`E081-V53
`E081-V54
`081-V55
`081-V56
`081-V57
`081-V58
`081-V59
`081-V60
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`————-———=:—
`
`148
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`it‘ done make X
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`60,2“
`,1 Load blocks accordingtablclz till I6. WcLiug‘l/indncrancc
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`EK
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`——_— £ —
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`J/_:_ .8_ J
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`Exeriment
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`0.4351
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`L 5
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`’:
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`090909-0xE08l-V37
`till V44
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`09sep09
`090909-0xE081-V49
`till V56
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`5
`87.58
`
`5
`87.02
`
`Reviewed by
`
`
`
`‘EDS: __ Date __—————9O3'0” ‘ 10° ‘°
`
`149