`
`Exhibit 2009
`E.I. du Pont de Nemours & Co. and
`Acher-Daniels-Midland Co. v. Furanix Technologies BV
`IPR2015-01838
`
`
`
` ‘tal REMARK:
`
`Date weighing, diluting Cat’s
`
`Date weighing, diluting Cat’s
`
`Date weighing, dissolving substrate
`
`Date starting reaction of experiment
`
`Date weighing, dissolving and adding Saccharine stock solution :
`
`Date of analyzing with the HPLC
`
`HPLC-analyzing according HPI.C—6 loghoek
`
`Experimental
`if done make X
`
`Thad blodrs according Iable12 till 16. Weighing tolaance‘
`jlkdd slitting nngnet and cap with Avamium disk 11352955. These caps leaked so old ones “Big” used.
`Close the blocks according OP-CI-I-100: Manual I-IPHPQCS.
`Biing ondapxessute with gun 20 Bar at RT according OP-CH-99: Pressntiser Work pmcedote
`Placinpieheatedl-l'I'HPQCS#LR-041 of 160 or 180 “C accordingsettingsinlable2,du|ing l or 0.5 hours.
`Fill in logbodnm: HTHPQCS-E13
`Plaoeinnnediatelyafiu-thexeactiontimeinanicebafl1d1ning30mimnes_
`jopen and thereby decompress reactors in a fumdiood.
`
`TIansfetethesedihitionsto7timesto8mlvialswithPastan'spipettes_
`
`Dilute700timesby10|dofdiludm1s78fimes+990plofWatefinHPICvials.
`
`Table 4: Substrate NIl\/IF solutions. in table 11 to 26
`
`S01 B HNIFIANIF
`
`Amount
`
`113.34 II 1 ml
`AMF
`53.34
`.-_
`— —
`HMF[sl
`[60ma/ml]
`
`
`%———
`
`ion (ms/ml)
`m
`22
`- "‘°"“"“"““"“ 2
`
`8
`
`‘ii
`
`I —
`
`2
`
`
`
`
`
`
`87.58
`
`5
`87.02
`
`090909-0xE08l -V37
`till V44
`
`095423309
`090909-0xE08 l-V49
`till V56
`
`S01 F DNIF
`7622 H 1 ml
`
`for F-I
`
`—
`
`Amount
`for F-2
`03307
`
`5.0
`76-14
`
`090910-0xE081-V45
`till V48
`
`090909-0xE081-V57
`till V60
`
`Table 10: List of catalysts.
`
`EEEEEEIEIIEZI C0Ac 411:0
`
`411:0 Tr Br/Co+Mn
`
`E EE£lEj
`
`Elfllflllflj
`EEEEEE
`I I
`
`3
`
`
`
`Table 11: Block 1 Blocknr:
`
`/remp =2 I P= 20 bar (An) / T.,=
`
`‘
`
`Efifi
`-—-Ml--MI-‘
`Iizfljfilj:
`“mg-
`Zfijj
`EH11“
`Em
`Kiln
`jljfiljg
`Zn”:-
`lfljiijjj
`Ifiljiljfilz:
`[E112-
`-1:21
`
`Table 12: Block 1 Blocknr:
`/Temp =
`I P: 20 bar (An) / 11;
`Efifi
`-—-fl---EI--
`EIZ1j=
`mg-
` E—jj
`Eljljfiln
`“Em-
` Z—n
`nun};
`II HMWAMF (3/2)
`0-5"-13 Em 0xE°81-V20
`KI
`HMFIAMF
`3
`0.5mlC Em 0xE08l—V2l
`IE]
`HMF/AMF
`3
`0.5 ml C 112: 0xE08l-V22
`IZ 0-51-1113 XI“ 0xE°81-V23
`T 0.5mlD Em 0xE081—V24
`
`Table 13: Block 3 Blocknr: /Temp=2 I P: 20 bar (An) /T0: ‘
`
`E@% ‘.‘.1’:.f
`-—-E[l‘EI--
` Zm
`zflifiln
`Z112:
`Iifilljj
`Ia:
`KICK“
`Tfilljj
`II“ °-5m1D Ia: 0xE°8l-V32
`II-Ijfiifilfg 0xE08l-V33
`III“ 0511115 Em 0xE081-V34
`Enilin 0313031-V35
`
` Z1n 0xE08l-V36
`
`Table 14; Block 4 Blocknr: /Temp =2 / p: 20 bar (Air) / T.,=
`
`d_d_:9sep09 ‘
`
`Bfifl
`2—2E[_‘IE1III‘
`- 0—5m1F-1 Em: 0xE08l—V37
`
`j_ 0-5n-IF-1 Im 0xE08l-V38
`
`4
`
`
`
`OO
`
`2E2
`
`081-V49
`081-V50
`081-V51
`081-V52
`081-V53
`081-V54
`081-V55
`081-V56
`081-V57
`081-V58
`081-V59
`081-V60
`
`N."-’NEHHI
`
`E
`
`Catalysts:
`
`fl
`
`Table 14: Block 5 Blocknr: rremp =2 I P: so bar (Air) /T —
`
`d.d..: l0sep09 -
`
`ZTIEIII
`Kizifizlflflfi
`1
`Iijfiiflfllfl
` I
`E °"4"“"‘
` ‘
`
`T‘ eggs§§as
`ogeg§5st IIIIIEIEE
`NN Q2922E§§§oaseaé
`iiiiiiiiiiiilfi
`
`
`5
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