`
`- Aurora
`
`“gill/Analytics
`
`Innovative Chemistry. Neeteric Solutions.
`
`Certificate of Analysis
`
`
`1 Product Name:
`
`Compound 13 Darunavir, isopropanol
`
`recrystallized
`
`
`
`Product Number:
`
`Lot Number:
`
`C13-040415-l
`
`Amount:
`Chemical Name:
`
`CAS Number:
`
`0.4 g
`[(1 8,2R)-3-[[(4-aminophenyl)sulfonyl](2-methylpropyl)amino]-2—
`hydroxy~i~ (phenylmethyl)propyl]-carbamic acid (3R,3aS,6aR)-
`hexahydrofuro[2,3-b] furan-B-yl ester
`20631-99-1
`
`Chemical Formula:
`
`C27H37N30rS
`
`Molecular Weight:
`
`547.66 gfmole
`
`Structure:
`
`on
`
`‘/J\CH3
`
`H
`
`O
`
`L
`
`Compound 13, Darunavir
`
`
`
`Appearance:
`
`Very fine powder (recrystallized from
`isopropanol)
`97%
`Purity (HPLC-UVm):
`101-104 °C
`Mp (°C, uncorrected)
`Consistent with structure
`NMR(CDC13)
`Consistent with molecular formula
`LRMS (ESI+)
`EtOAc, DCM, ethanol
`Solubility:
`NA
`TLC (Silica gel 60 F254)
`
`Stora e:
`2-8 °C_. protect from light and moisture
`
`
`Certified by:
`
` Chic Operating Officer
`
`
`
`Date:
`
`L” a”;
`
`Aurora Analytics. LLC
`[450 South Rolling Road
`Baltimore, MD 2122?
`
`Phone: 443-543-5?99
`FAX: 443-543-5790
`akalivret@auroraanalyticscom
`Lupin Ex. 1091 (Page 1 of 1)
`Lupin Ex. 1091 (Page 1 of 1)
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