`-- llAnalytlcs
`
`innovative Chemistry. Neoteric Solutions.
`
`Certificate of Analysis
`
`
`Product Name:
`Product Number:
`
`Compound 13 Darunavir, ethanol recrystallized
`
`Lot Number:
`
`C13-040415-E
`
`
`
`Amount:
`Chemical Name:
`
`CAS Number:
`
`0.5 g
`[(1S,2R)—3-[[(4-aminophenyl)sulfonyl](2—methylpropyl)amino]-2—
`hydroxy-l- (phenylmethyl)propyl]—carbamic acid (3R,3aS.6aR)-
`hexahydrofuro[2,3-b]furan—3-yl ester
`20631-99—1
`
`Chemical Formula:
`
`C27H37N3078
`
`Molecular Weight:
`
`54?.66 g/mole
`
`Structure:
`
`CH3
`
`9H H\CH3
`
`3'
`
`H
`
`
`
`
`Compound 13, Darunavir
`
`
`Appearance:
`
`Purity (HPLC-Usta):
`Mp (°C, uncorrected)
`NMR (CDCIJ)
`LRMS (ESI+)
`Solubility:
`TLC (Silica gel 60 F254)
`Storage:
`
`Certified by:
`
`Very fine powder (recrystallized from
`Ethanol)
`97.5%
`93-96 °C
`Consistent with structure
`Consistent with molecular formula
`EtOAc, DCM, ethanol
`NA
`
`2-8 “C, protect from light and moisture
`
`Chief Operating Officer
`
`Date:
`
`2! 6(LS
`
`Aurora Analytics, LLC
`1450 South Rolling Road
`Baltimore, MD 2 l2?
`
`-
`
`Phone: 4436436799
`FAX: 443-543-5790
`akalivret@auroraanalytics.com
`Lupin Ex. 1090 (Page 1 of 1)
`Lupin Ex. 1090 (Page 1 of 1)
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