IN THE UNITED STATES PATENT AND TRADEMARK OFFICE
`
`BEFORE THE PATENT TRIAL AND APPEAL BOARD
`
`ENZYMOTEC LTD.,
`Petitioner
`
`v.
`
`NEPTUNE TECHNOLOGIES AND BIORESSOURCES INC.,
`Patent Owner
`
`IPR2014-00556
`
`ENZYMOTEC LTD.’S UPDATED EXHIBIT LIST
`
`Mail Stop “PATENT BOARD”
`Patent Trial and Appeal Board
`United States Patent and Trademark Office
`P.O. Box 1450
`Alexandria, VA 22313-1450
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`BEFORE THE PATENT TRIAL AND APPEAL BOARD
`
`ENZYMOTEC LTD.,
`Petitioner
`
`v.
`
`NEPTUNE TECHNOLOGIES AND BIORESSOURCES INC.,
`Patent Owner
`
`IPR2014-00556
`
`ENZYMOTEC LTD.’S UPDATED EXHIBIT LIST
`
`Mail Stop “PATENT BOARD”
`Patent Trial and Appeal Board
`United States Patent and Trademark Office
`P.O. Box 1450
`Alexandria, VA 22313-1450
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`ENZYMOTEC
`EXHIBIT
`1001
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`Case No. IPR2014-00556
`Enzymotec Ltd.’s Updated Exhibit List
`
`DESCRIPTION
`U.S. Pat. No. 8,278,351 to Sampalis (“’351”)
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`WO 00/23546 to Beaudoin (“Beaudoin I”)
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`Canadian Application 2,251,265 to Beaudoin (“Beaudoin II”)
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`Certified translation of Ex. 1070: Japanese Unexamined Patent
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`Application Publication No. 02-215351, titled Krill
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`Phospholipids Fractioning Method (“Maruyama,”); Certificate
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`of Translation provided as Ex. 1071.
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`Certified translation of Ex. 1072: Fisheries Agency, General
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`Report on Research and Development of Techniques in
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`Processing and Utilization of Marine Products, Chapter 6,
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`Development of technology for recovery of valuable substances
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`(astaxanthin) from krill, by Takao Fujita, pp. 273-307 (March
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`1985) (“Fujita”) ; Certificate of Translation provided as Ex. 1073.
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`Fricke et al., Lipid, Sterol, and Fatty Acid Composition of
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`Antarctic Krill, Lipids, Vol. 19, No. 11, pp. 821-827 (1984)
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`(“Fricke”)
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`1
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`1002
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`1003
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`1004
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`1005
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`1006
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`ENZYMOTEC
`EXHIBIT
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`1007
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`1008
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`1009
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`1010
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`1011
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`1012
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`Case No. IPR2014-00556
`Enzymotec Ltd.’s Updated Exhibit List
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`DESCRIPTION
`Bottino, N.R., “Lipid Composition of Two Species of
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`Antarctic Krill: Euphausia Superba and E. Crystallorophias,”
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`Comp. Biochem. Physiol., 1975, Vol. 50B, pp. 479-484
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`(“Bottino”)
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`Canadian Patent No. 1098900, titled Method for the Processing
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`of Krill to Produce Protein, Lipids and Chitin (“Rogozhin”)
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`Itano Refrigerated Food Co., Ltd., Bio & High Technology
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`Announcement and Natural Astaxanthin & Krill Lecithin, pp. 1-
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`16 (on or before December 28, 1994) (“Itano”)
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`WO97/39759 to Stoll (“Stoll”)
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`Final Prospectus dated May 11, 2001 (“Final Prospectus”)
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`“Neptune Technologies & Bioressources Soon to Obtain a Major
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`Patent in Over 30 Countries” (“2011 Press Release,”)
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`Le Grandois et al., Investigation of Natural Phosphatidycholine
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`Sources: Separation and Identification by Liquid
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`1013
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`Chromatography -Electrospray Ionization-Tandem Mass
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`Spectrometry (LC-ESI- MS2) of Molecular Species, J. Agric.
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`Food Chem., 57, 6014-20 (2009) (“Le Grandois”)
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`2
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`ENZYMOTEC
`EXHIBIT
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`1014
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`1015
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`1016
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`1017
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`1018
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`1019
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`Case No. IPR2014-00556
`Enzymotec Ltd.’s Updated Exhibit List
`
`DESCRIPTION
`Certified translation of Ex. 1074: Japanese Patent No. 60-
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`153779, entitled “Nutritional Supplement” (“Fukuoka ”);
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`Certificate of Translation provided as Ex. 1075
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`Certified translation of Ex. 1076: Japanese Patent Publication
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`No. H08-231391, entitled “Medicine for Improvement of
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`Dementia Symptoms” (“Yasawa”); Certificate of Translation
`
`provided as Ex. 1077.
`
`Suzuki, T. and Shibata, N., “The utilization of Antarctic krill
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`for human food,” Food Rev. Int’l, 6:1, 119-147 (1990)
`
`(“Suzuki”)
`
`Bergelson (ed.), Lipid Biochemical Preparations, Chapter I.1, pp.
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`1-13 (1980) (“Bergelson”)
`
`WHO News and Activities, Bulletin of the World Health
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`Organization, 73(4), pp. 547-51 (1995) (“WHO Bulletin”)
`
`Bell and Dick, Molecular Species Composition of the Major
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`Diacyl Glycerophospholipids from Muscle, Liver, Retina and
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`Brain of Cod (Gadus morhua), Lipids, Vol. 26, No. 8, pp. 565-
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`573 (1991) (“Bell and Dick”)
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`3
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`ENZYMOTEC
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`1020
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`1021
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`1022
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`1023
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`1024
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`1025
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`Case No. IPR2014-00556
`Enzymotec Ltd.’s Updated Exhibit List
`
`DESCRIPTION
`Henderson et al., Lipid Composition of the Pineal Organ from
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`Rainbow Trout (Oncorhynchus mykiss), Lipids, Vol. 29, No.
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`5, pp. 311-317 (1994) (“Henderson ”)
`
`Bell, Molecular Species Analysis of Phosphoglycerides from the
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`Ripe Roes of Cod, Lipids, Vol. 24, No. 7 (1989)
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`Takahashi et al., Compositional Changes in Molecular Species of
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`Fish Muscle Phosphatidylcholine During Storage, Bull. Fac. Fish.
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`Hokkaido Univ. 37(1), 80-84 1986.
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`Takahashi et al., Prediction of Relative Retention Value of the
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`Individual Molecular Species of Diacyl Glycerolipid on High
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`Performance Liquid Chromatography, Bull. Fac. Fish.
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`Hokkaido Univ. 38(4), 398-404. 1987
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`Lin et al., Effect of Dietary N-3 Fatty Acids Upon the
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`Phospholipid Molecular Species of the Monkey Retina,
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`Invest Ophthalmol Vis Sci. 1994;35:794-803
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`Farkas, Composition and Physical State of Phospholipids in
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`Calanoid Copepods from India and Norway, LIPIDS, Vol. 23,
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`No. 6 (1988)
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`4
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`ENZYMOTEC
`EXHIBIT
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`1026
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`1027
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`1028
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`1029
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`1030
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`Case No. IPR2014-00556
`Enzymotec Ltd.’s Updated Exhibit List
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`DESCRIPTION
`Bell, Molecular Species Composition of Phosphatidylcholine
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`from Crypthecodinium cohnii in Relation to Growth Temperature
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`Lipids 25, 115-118 (1990)
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`Buda, Structural order of membranes and composition of
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`phospholipids in fish brain cells during thermal
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`acclimatization, Proc. Natl. Acad. Sci. USA Vol. 91, pp. 8234-
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`8238, August 1994
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`Takahashi et al., Molecular Species of Fish Muscle Lecithin,
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`Bulletin of the Japanese Society of Scientific Fisheries
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`48(12), 1803-1814 (1982)
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`Tocher, Chapter 6, Glycerophospholipid metabolism,
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`Biochemistry and molecular biology of fishes, vol. 4,
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`Hochachka and Mommsen (eds.)(1995)
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`Tanaka, Biosynthesis of 1,2-dieicosapentaenoyl-sn-glycero-3-
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`phosphocholine in Caenorhabditis elegans, Eur. J. Biochem.
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`263, 189±194 (1999)
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`5
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`ENZYMOTEC
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`1031
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`1032
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`1033
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`1034
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`1035
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`1036
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`1037
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`1038
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`1039
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`Case No. IPR2014-00556
`Enzymotec Ltd.’s Updated Exhibit List
`
`DESCRIPTION
`Winther et al., Elucidation of Phosphatidylcholine Composition
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`in Krill Oil Extracted from Euphausia superba, Lipids 46(1):25-
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`36 (2011)(“Winther”)
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`Eichberg, “Lecithin – It Manufacture and Use in the Fat and Oil
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`Industry,” Oils and Soap 51-54, 1939 (“Eichberg”)
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`Balassa et al., Microencapsulation in the Food Industry, Critical
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`Reviews in Food Technology, 2:2, 245-265 (1971)(“Balassa”)
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`Buchi R-220 Rotovapor® Manual
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`Johnson and Lucas, Comparison of Alternative Solvents for Oils
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`Extraction, JAOCS 60(2):229-242 (1983)
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`U.S. Pat. No. 4,714,571
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`Grit et al., Int. J. Pharmaceutics 50:1-6 (1989)
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`Herman and Groves, Pharmaceutical Research 10(5):774-
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`776 (1993)
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`Watanabe et al., Effective Components in Cuttlefish Meal
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`and Raw Krill for Improvement of Quality of Red Seabream
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`Pagrus major Eggs, Nippon Suisan Gakkaishi 57(4):681-694
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`(1991)(“Watanabe”)
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`ENZYMOTEC
`EXHIBIT
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`1040
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`1041
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`1042
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`1043
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`1044
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`1045
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`1046
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`Case No. IPR2014-00556
`Enzymotec Ltd.’s Updated Exhibit List
`
`DESCRIPTION
`Declaration of Dr. Richard van Breemen in Support of Inter
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`Partes Review of U.S. Pat. No. 8,278,351 (“Van Breemen”)
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`Declaration of Dr. Suzanne Budge in Support of Inter Partes
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`Review of U.S. Pat. No. 8,278,351 (“Budge”)
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`Declaration of Dr. Thomas Brenna in support of Inter Partes
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`Review of U.S. Pat. No. 8,278,351
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`Expert Witness Report of Dr. Theodore Welch submitted
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`in relation to ITC Investigation No. 337-TA-877
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`(“Welch”)
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`Declaration of Dr. Jeff Moore in Support of Inter Partes Review
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`of U.S. Pat. No. 8,278,351 (“Moore”)
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`Declaration of Dr. Albert Lee in Support of Inter Partes Review
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`of U.S. Pat. No. 8,278,351 (“Lee”)
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`Declaration of Dr. Ivar Storrø in support of Inter Partes Review
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`of U.S. Pat. No. 8,278,351 (“Storrø”)
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`7
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`Case No. IPR2014-00556
`Enzymotec Ltd.’s Updated Exhibit List
`
`DESCRIPTION
`Declaration of Bjorn Ole Haugsgjerd submitted during inter
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`partes reexamination of parent patent U.S. 8,030,348
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`(“Haugsgjerd ‘348
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`Decl.”)
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`Supplemental Declaration of Bjorn Ole Haugsgjerd submitted
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`during inter partes reexamination of parent patent U.S.
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`8,030,348 (“Haugsgjerd ‘348 Supp. Decl.”)
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`Declaration of Dr. Thomas Gundersen submitted during inter
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`partes reexamination of parent patent U.S. 8,030,348
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`(“Gundersen Decl.”)
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`Supplemental Declaration of Dr. Thomas Gundersen submitted
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`during inter partes reexamination of parent patent U.S.
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`8,030,348 (“Gundersen Supp. Decl.”)
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`Declaration of Dr. Earl White submitted during prosecution
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`of parent patent U.S. 8,030,348 (“2011 White Decl.”)
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`Supplemental Declaration of Dr. Earl White submitted during
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`prosecution of parent patent U.S. 8,278,351 (“White Supp.
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`Decl.”)
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`8
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`ENZYMOTEC
`EXHIBIT
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`1047
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`1048
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`1049
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`1050
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`1051
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`1052
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`1053
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`1054
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`1055
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`1056
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`1057
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`1058
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`Case No. IPR2014-00556
`Enzymotec Ltd.’s Updated Exhibit List
`
`DESCRIPTION
`Declaration of Dr. Jacek Jaczynski from inter partes
`
`reexamination of the parent patent U.S. 8,030,348 (“Jaczynski
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`Reexam. Decl.”)
`
`Declaration of Dr. Yeboah submitted during inter partes
`
`reexamination of parent patent U.S. 8,030,348 (“Yeboah
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`Reexam Decl.”)
`
`Supplemental Declaration of Dr. Earl White submitted during
`
`inter partes reexamination of parent patent U.S. 8,030,348
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`(“White
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`Supp. Reexam. Decl.”)
`
`Declaration of Dr. Shahidi submitted during inter partes
`
`reexamination of parent patent U.S. 8,030,348 (Shahidi
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`Reexam. Decl.”
`
`Declaration of Dr. Tina Sampalis submitted during inter
`
`partes reexamination of parent patent U.S. 8,030,348
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`(Sampalis”)
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`Declaration of Dr. Yeboah submitted during prosecution of
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`parent patent U.S. 8,278,351 (“Yeboah ‘351 Decl.”)
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`9
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`Case No. IPR2014-00556
`Enzymotec Ltd.’s Updated Exhibit List
`
`DESCRIPTION
`Declaration of Dr. Shahidi submitted during prosecution of
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`parent patent U.S. 8,278,351 (Shahidi ‘351 Decl.”)
`
`Declaration of Dr. Jaczynski submitted during prosecution
`
`of parent patent U.S. 8,278,351 (Jaczynski ‘351 Decl.”)
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`April 2, 2012 Response to Office Action, ‘351 patent
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`Provisional Application No. 60/307,842 (Priority document for
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`the ‘351 patent)
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`Office Action dated January 5, 2012, ‘351 patent
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`Action Closing Prosecution, ‘348 patent
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`Grant of Request for Ex parte Reexamination of the ‘351 patent
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`Declaration of Dr. Van Breemen submitted during Ex parte
`
`Reexamination of the ‘351 patent (Van Breemen ‘351
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`Reexam. Decl.”
`
`Declaration of Dr. Van Breemen submitted during Inter
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`partes Reexamination of the ‘348 patent (Van Breemen ‘348
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`Reexam Decl.”
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`Medina et al., J. Amer. Oil Chem. Soc. 71(5):479-82 (1994)
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`U.S. Patent No. 8,030,348
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`ENZYMOTEC
`EXHIBIT
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`1059
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`1060
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`1061
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`1062
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`1063
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`1064
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`1065
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`1066
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`1067
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`1068
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`1069
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`ENZYMOTEC
`EXHIBIT
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`1070
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`1071
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`1072
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`Case No. IPR2014-00556
`Enzymotec Ltd.’s Updated Exhibit List
`
`DESCRIPTION
`Japanese Unexamined Patent Application Publication No. 02-
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`215351, titled Krill Phospholipids Fractioning Method; Japanese
`
`language document
`
`Certification of translation of Ex. 1070: Japanese Unexamined
`
`Patent Application Publication No. 02-215351
`
`Fisheries Agency, General Report on Research and
`
`Development of Techniques in Processing and Utilization of
`
`Marine Products, Chapter 6, Development of technology for
`
`recovery of valuable substances (astaxanthin) from krill, by
`
`Takao Fujita, pp. 273-307 (March 1985); Japanese language
`
`document
`
`Certificate of translation of Ex. 1072: Fisheries Agency, General
`
`Report on Research and Development of Techniques in
`
`Processing and Utilization of Marine Products, Chapter 6,
`
`1073
`
`Development of technology for recovery of valuable substances
`
`(astaxanthin) from krill, by Takao Fujita, pp. 273-307 (March
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`1985); Japanese language document
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`11
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`ENZYMOTEC
`EXHIBIT
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`1074
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`1075
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`1076
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`1077
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`1078
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`1079
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`1080
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`Case No. IPR2014-00556
`Enzymotec Ltd.’s Updated Exhibit List
`
`DESCRIPTION
`Japanese Patent No. 60-153779, entitled “Nutritional
`
`Supplement”; Japanese language document
`
`Certificate of translation of Ex. 1074: Japanese Patent No. 60-
`
`153779, entitled “Nutritional Supplement”
`
`Japanese Patent Publication No. H08-231391, entitled
`
`“Medicine for Improvement of Dementia Symptoms”; Japanese
`
`language document
`
`Certificate of translation of Ex. 1076: Japanese Patent
`
`Publication No. H08-231391, entitled “Medicine for
`
`Improvement of Dementia Symptoms”
`
`Folch, et al., A Simple Method for the Isolation and Purification
`
`of Total Lipids from Animal Tissues. J. Biol. Chem., 226, 497-
`
`509 (1957)
`
`Declaration of Dr. Chong Lee submitted during inter partes
`
`reexamination of parent patent U.S. 8,030,348 (“Yeboah
`
`Reexam Decl.”)
`
`Declaration of Bjorn Ole Haugsgjerd in support of Inter Partes
`
`Review of U.S. Pat. No. 8,278,351 (“Haugsgjerd”)
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`12
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`Case No. IPR2014-00556
`Enzymotec Ltd.’s Updated Exhibit List
`
`
`ENZYMOTEC
`EXHIBIT
`
`DESCRIPTION
`Declaration of Daniel P. Margolis in Support of Motion for Pro
`
`1081
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`Hac Vice Admission Under 37 C.F.R. § 42.10(c)
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`Dated: May 30, 2014
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`Respectfully submitted,
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`/Elizabeth J. Holland/
`Elizabeth J. Holland (Reg. No. 47,657)
`Cynthia Lambert Hardman (Reg. No. 53,179)
`KENYON & KENYON LLP
`One Broadway
`New York, NY 10004-1007
`Tel: (212) 425-7200
`Fax: (212) 425-5288
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`Counsel for Petitioner Enzymotec Ltd.
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`13
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