`______________________
`
`BEFORE THE PATENT TRIAL AND APPEAL BOARD
`______________________
`
`
`
`AKER BIOMARINE AS and ENZYMOTEC LTD.
`Petitioners
`
`v.
`
`NEPTUNE TECHNOLOGIES AND BIORESSOURCES INC.
`Patent Owner
`
`______________________
`
`CASE IPR2014-000031
`U.S. Patent No. 8,278,351
`______________________
`
`
`
`NEPTUNE TECHNOLOGIES AND BIORESSOURCES INC.’S
` UPDATED EXHIBIT LIST
`
`
`
`
`
`
`1 Case IPR2014-00556 has been joined with this proceeding.
`
`
`
`
`
`
`Neptune Updated Exhibit List
`Case No. IPR2014-00003/IPR2014-00556
`
`
`BRIEF DESCRIPTION
`
`NEPN EXHIBIT
`NO.
`NEPN 2001
`
`NEPN 2002
`
`NEPN 2004
`
`NEPN 2005
`
`Excepts from the rebuttal witness statement of Dr. Jacek Jaczynski,
`prepared for International Trade Commission Investigation No. 337-TA-
`877 (“Jaczynski Rebuttal Witness Statement” or “Jaczynski Stmnt”)
`Enzymotec document, titled “Introduction to Multi Stage Oil Extraction
`Process.” (“Enzymotec Extraction”)
`NEPN 2003 Material Safety Data Sheet (MSDS) for denature ethanol (“MSDS
`Ethanol”)
`Pages from Solomons and Fryhle, Organic Chemistry, 7th ed., J. Wiley,
`2000, (“Solomons and Fryhle”)
`Declaration of Dr. Richard Charles Oppenheim submitted by the Petitioner
`during the opposition of AU Patent No. 2002322233, (“Oppenheim
`Declaration”)
`NEPN 2006 Medina et al., “C Nuclear magnetic resonance monitoring of free fatty acid
`release after fish thermal processing,” J. Amer. Oil Chem. Soc. 71(5):
`479-482 (1994) (“Medina”)
`Bruheim, et al. U.S. Patent Publication No. 2011/0104297, titled
`“Methods of Using Krill Oil to Treat Risk Factors for Cardiovascular,
`Metabolic, and Inflammatory Disorders.”
`Neptune GRAS notice of January 18, 2008 (“Neptune Gras Notice”)
`Aker GRAS notice of December 14, 2010 (“AKER Gras Notice”)
`Enzymotec GRAS notice of May 26, 2007 (“Enzymotec 2007 Gras
`Notice”)
`Enzymotec GRAS notice of December 14, 2009 (“Enzymotec 2009 Gras
`Notice”)
`Yamaguchi et al., Supercritical Carbon Dioxide Extraction of Oils from
`Antarctic Krill, J. Agric. Food Chem. 1988 (“Yamaguchi”)
`NEPN 2013 Material Safety Data Sheet (MSDS) for methanol (“MSDS Methanol”)
`NEPN 2014 Material Safety Data Sheet (MSDS) for chloroform (“MSDS Chloroform”)
`
`
`NEPN 2007
`
`NEPN 2008
`NEPN 2009
`NEPN 2010
`
`NEPN 2011
`
`NEPN 2012
`
`
`
`2
`
`
`
`Neptune Updated Exhibit List
`Case No. IPR2014-00003/IPR2014-00556
`
`
`BRIEF DESCRIPTION
`
`NEPN EXHIBIT
`NO.
`NEPN 2015
`
`NEPN 2016
`
`NEPN 2017
`
`NEPN 2018
`
`NEPN 2019
`
`File History of U.S. 6,800,299 (U.S.S.N. 09/830,146), Office Action
`Response of August 25, 2003. (“‘299 Patent Office Action Response”)
`S. Garcia and R. Grainger, "Gloom and doom? The future of marine
`capture fisheries", Phil. Trans. R. Soc., Vol. 360 pp. 21-46 (“Garcia”)
`Declaration of Laura Cunningham in Support of Motion to Appear Pro Hac
`Vice on Behalf of Patent Owner Neptune
`Transcript of telephonic conference call before the Patent Trial and
`Appeal Board, April 25, 2014
`Declaration of Jonathan G. Graves in Support of Motion to Appear Pro
`Hac Vice on Behalf of Patent Owner Neptune
`X. Liping, S. Mjos and B.Haugsgjerd “Efficiencies of three common lipid
`extraction methods evaluated by calculating mass balances of the fatty
`acids”, J. Food Composition and Analysis (2012) 198-197
`Intentionally Omitted
`Transcript of telephonic conference call before the Patent Trial and
`Appeal Board, May 13, 2014
`The public version of the Aker Respondents’ Opposition to Complainants’
`Motion to Compel the Aker Respondents and Related Third-Parties to
`Produce All Responsive Documents and Testimony Related to
`Reexamination Testing, September 18, 2013
`Excerpts from the deposition transcript of Bjorn Ole Haugsgjerd, May 21,
`2014
`Email exchange between Laura Cunningham and Leslie M. Schmidt, May
`26, 2014
`Rough Transcript of telephonic conference call before the Patent Trial and
`Appeal Board, May 28, 2014
`Transcript of telephonic conference call before the Patent Trial and
`Appeal Board, May 28, 2014
`Seafoodplus – New lipid oxidation method
`NEPN 2028
`NEPN 2029 October 11, 2013 Deposition of James Brenna, ITC Inv. No. 337-TA-877
`
`NEPN 2020
`
`NEPN 2021
`NEPN 2022
`
`NEPN 2023
`
`NEPN 2024
`
`NEPN 2025
`
`NEPN 2026
`
`NEPN 2027
`
`
`
`3
`
`
`
`Neptune Updated Exhibit List
`Case No. IPR2014-00003/IPR2014-00556
`
`
`NEPN EXHIBIT
`NO.
`
`BRIEF DESCRIPTION
`
`(excerpts)
`Translated Beaudoin Laboratory Notebook
`NEPN 2030
`Translated Beaudoin Laboratory Notebook
`NEPN 2031
`Beaudoin Laboratory Notebook Pages in French
`NEPN 2032
`Protective Order
`NEPN 2033
`Beaudoin Laboratory Notebook Pages in French
`NEPN 2034
`NEPN 2035 May 21, 2014 Deposition Transcript of Bjorn Haugsgjerd
`NEPN 2036
`US Patent No. 4,714,571, Tremblay
`NEPN 2037
`June 4, 2014 Deposition Transcript of James Brenna
`NEPN 2038
`June 5, 2014 Deposition Transcript of Ivan Storro
`NEPN 2039
`June 6, 2014 Deposition Transcript of Suzanne Budge
`NEPN 2040
`Aker webpage, “The Phospholipid Advantage”
`NEPN 2041
`Enzymotec Introduction to Extraction Process
`NEPN 2042
`U.S. Patent 6,521,768, “Process for the Extraction of Lipids From Fatty
`Bird Tissues” (filed 11/09/2001)
`NEPN 2043 Gigliotti et al., “Extraction and characterisation of lipids from Antarctic krill
`(Euphausia superba),” 125 Food Chem. 1028-1036, 1031 (2011)
`Beaudoin US 6,800,299 Prosecution History
`Intentionally Omitted
`Benzene Material Safety Data Sheet
`Nicol et al. Krill: Biology, Ecology and Fisheries, Chapter 10 Products
`Derived from Krill
`Yoshitomi, “Utilization of Antarctic Krill for Food and Feed”, More Efficient
`Utilization of Fish and Fisheries Products, 2004
`Haugsgjerd Laboratory Notebook Translated AKBM_IPR0000001-36
`NEPN 2049
`Haugsgjerd Laboratory Notebook AKBM_IPR0000001-36
`NEPN 2050
`NEPN 2051 Oct. 2011 Lipid Extraction AKBM_IPR0000037-49
`
`NEPN 2044
`NEPN 2045
`NEPN 2046
`NEPN 2047
`
`NEPN 2048
`
`
`
`4
`
`
`
`Neptune Updated Exhibit List
`Case No. IPR2014-00003/IPR2014-00556
`
`
`BRIEF DESCRIPTION
`
`April 2012 Lipid Extraction AKBM_IPR0000050-71
`Results of Analysis AKBM_IPR0000072
`Results of Analysis AKBM_IPR0000073
`Budge Notebook AKBM_IPR0000074-87
`Bunea, Evaluation of the effects of Neptune Krill oil on the clinical course
`of hyperlipidemia; Alternative Medicine Review 2004; 9(4):420-428
`Deutsch, Evaluation of the effects of Neptune Krill Oil on chronic
`inflammation and arthritic symptoms, Journal of American College of
`Nutrition, Vol. 26, No. 1, 39-48 (2007)
`Sampalis F, Bunea R, Pelland MF, Kowalski O, Duguet N, and Dupuis S.,
`Evaluation of the Effects of Neptune Krill Oil on the Management of
`Premenstrual Syndrome, Alternative Medicine Review 8(2):171-9 (2003)
`Declaration of Jacek Jaczynski
`Fats & Oils: Practical Guides for the Food Industry (excerpts), 1996
`Supplemental Declaration of Jacek Jaczynski
`ITC Witness Statement of Dr. David Pond – Excerpts
`Transcript of telephonic conference call before the Patent Trial and
`Appeal Board, June 12, 2014
`Transcript of telephonic conference call before the Patent Trial and
`Appeal Board, August 26, 2014
`September 23, 2014 email from Laura Cunningham
`Patent Owner’s Demonstrative Exhibits
`
`
`
`5
`
`NEPN EXHIBIT
`NO.
`NEPN 2052
`NEPN 2053
`NEPN 2054
`NEPN 2055
`NEPN 2056
`
`NEPN 2057
`
`NEPN 2058
`
`NEPN 2059
`NEPN 2060
`NEPN 2061
`NEPN 2062
`NEPN 2063
`
`NEPN 2064
`
`NEPN 2065
`NEPN 2066
`
`
`
`
`
`
`
`Neptune Updated Exhibit List
`Case No. IPR2014-00003/IPR2014-00556
`
`
`Respectfully submitted,
`COOLEY LLP
`
`/ J. Dean Farmer /
`J. Dean Farmer, Ph.D.
`Reg. No. 59,917
`
`
`
`
`
`
`By:
`
`
`
`
`Dated: October 30, 2014
`
`COOLEY LLP
`ATTN: Patent Group
`1299 Pennsylvania Avenue, N.W
`Suite 700
`Washington, DC 20004-2400
`
`Tel: (617) 937-2371
`Fax: (202) 842-7899
`
`
`
`
`
`
`
`
`
`
`
`6
`
`
`
`Neptune Updated Exhibit List
`Case No. IPR2014-00003/IPR2014-00556
`
`
`Elizabeth J. Holland
`eholland@goodwinprocter.com
`Goodwin Procter LLP
`The New York Times Building
`620 Eighth Avenue
`New York, NY 10018
`Telephone: (212) 813-8800
`Facsimile: (212) 355-3333
`Reg. No. 47,657
`
`Cynthia Lambert Hardman
`chardman@goodwinprocter.com
`Goodwin Procter LLP
`The New York Times Building
`620 Eighth Avenue
`New York, NY 10018
`Telephone: (212) 813-8800
`Facsimile: (212) 355-3333
`Reg. No. 53,179
`
`
`
`Respectfully submitted,
`
`COOLEY LLP
`
`CERTIFICATION OF SERVICE UNDER 37 C.F.R. §§ 42.6(e), 42.205(b)
`I, J. Dean Farmer, Ph.D., hereby certify that the foregoing NEPTUNE UPDATED
`
`EXHIBIT LIST was served electronically (as consented to by Petitioners), on October 30,
`2014, the same day as the filing of the above-identified documents in the United States
`Patent and Trademark Office (USPTO), upon:
`
`Amanda Hollis
`amanda.hollis@kirkland.com
`Hand delivery address:
`KIRKLAND & ELLIS
`300 North LaSalle
`Chicago, IL 60654
`Telephone: 312-862-2011
`Facsimile: 312-862-2200
`Reg. No. 55,629
`
`J. Mitchell Jones
`jmjones@casimirjones.com
`docketing@casimirjones.com
`Hand delivery address:
`CASIMIR JONES SC
`2275 Deming Way, St. 310
`Middleton, WI 53562
`Telephone: (608) 662-1277
`Facsimile: (608) 662-1276
`Reg. No. 44,174
`
`Dated: October 30, 2014
`
`COOLEY LLP
`ATTN: Patent Group
`1299 Pennsylvania Avenue, N.W
`Suite 700
`Washington, DC 20004-2400
`Tel: (617) 937-2371
`Fax: (202) 842-7899
`
`
`/J. Dean Farmer/
`J. Dean Farmer, Ph.D.
`Reg. No. 57,917
`
`
`
`By:
`
`
`
`
`
`7