`
`St. Eeam “K1111 Gil gsraductiexa accmding E3
`the Beazuisiaa patent,” Natebmk mga,
`Negmme Tec11n0E<3gies & Bimegaurces
`(ZSG9)
`
`1
`
`1
`
`AKBM 1104
`
`AKBM 1104
`
`
`
`
`
`‘.4‘>‘3'¢?S€
`
`;'§eICS£.Q-i3f.§£ £8 iU€§~?3.£.S-S£3'<.."3?Cfi5
`
`Report R 3:. £3 activities it1'Nevember{)9
`Project: New marine Ettknttrtfi-S‘ & r3e.‘}ze:' p_r'oa"tec:rs
`Made by: Pierre St-jean
`
`Kriii {Bil preductitm aeeerding to the 36331630311 patent
`
`Methttdttiegy
`
`Extraetitm aceeraziitag to the Beatadeitt patent
`
`Step 1
`
`3 kg ofktiii split into ti X 5003;
`Add 6 volumes at‘ acetone
`
`Grind for 28 mitt.
`
`Extract for 12!} min. without agitation
`Iiiiiter
`Wash seiiti with 3 voiitmes of aeetette
`
`Combine the twfl fiittates
`
`Evap0ra§'.e the aceimte
`Separate the fat from the water by deeatttatieti after addititm of 1 volume of acetone
`Reezmr-ea‘ Oi}.
`
`E‘vap0rat.e under vac L! 1! m
`Pitt aside
`
`Step 2
`
`Extract frorn svaiiti with 2 volumes of ethane! 30 min at 4"‘(I
`Fiiter
`
`Combine with the fiitrate to the f"tt'..~;t oi}. extraction
`
`Evaperate under vacuum
`Heat at I25‘?
`
`Resttits
`
`The yield ofeii protiuetion. was more than fififig, The oi? is reddish brown anti it is very otiet‘ou.s.
`Extraction of kriii in the fitztt extraction gave a stable €1'I'EI_!i:-_ii01'2
`that we hati to ‘break by adding
`acetone to teciuee the voiume of water associated with the fat.
`
`2
`
`
`
`‘
`Ragpofi d’activité'§R&D novmlzbrc-2 09
`Projct : N014’ veiie I3.*0ma.s'3e marzmz &. aux:-'83 prodmrs
`: Picrrg St_j‘{:an
`
`
`_.
`
`g.
`“*-
`--
`-'
`"g"
`Ԥ-'
`rs-2;num_:‘:-:;:2s .2 s;:ms':'s:‘:-..-ar..«‘_s
`
`Prmiusctian cfiauifie tie ieriii scion ie brevei; de Beaudnin
`
`Nléihadalugie
`
`Extractiois 3230:: breve‘: Beaudain
`
`Etape 1
`
`3 kg 01-: kriii K31 RE fractiormés en 6 X 5€}£3g
`Ajmaicr 6 voiumt-:3 <.i’a<:é1'o.nc
`B;'0yc1' pendant 20 min.
`Extraire pendant 125 min. sans agitation
`Fiitrer
`
`Lava‘ Faquatéinc was 2 Voiuancs d'”acét0uc
`Combincr lcs deux fiiiira.ts
`Evaporer 1°a.cét0ne
`Eééparer ie gras tie i’eaa.1.par 1.'1éC3£1tflti0£‘! aprés ajout de 1 voiume d’acét0n-3
`Récupérrcr i"nu'E}c
`Evaporcr sous vidc
`Rése;'ve;'
`
`éltape. 2
`
`Extraim 1’aq_uatéine a.x.»‘ee;: 2 volumes iféthanai 30 min £1 4°C
`ii~"ii'rrer
`
`jcindrc lc fiitrat is. Fhuilc cit: la prcmiérc extraction
`Evapm'c1' sous Vida
`{Ih.a:.:ft'er 5‘: 125°C
`
`Résuitats
`
`Ifhuiie: est do coulsur mtan-rouge ct‘
`de plus dc 360g.
`L-C i'i.3i1dCm{2‘:’1’t dc produciiura efhuiltz a
`ciic c;~;tt1'és odoraaatc. L’ext1'acticm du KI} RE. a donné en prcmiérc cxtractian unit éanuisioal stabie
`(.31,-Son a (if: iariser par ajaut d’a.cét0ne pour réd uire Ee vralum-3 d'"e-an associé an gras.
`
`05 dé(:(’!?4.-|_5:‘d 2099
`3
`
`3
Accessing this document will incur an additional charge of $.
After purchase, you can access this document again without charge.
Accept $ Charge
Still Working On It
This document is taking longer than usual to download. This can happen if we need to contact the court directly to obtain the document and their servers are running slowly.
Give it another minute or two to complete, and then try the refresh button.
A few More Minutes ... Still Working
It can take up to 5 minutes for us to download a document if the court servers are running slowly.
Thank you for your continued patience.
This document could not be displayed.
We could not find this document within its docket. Please go back to the docket page and check the link. If that does not work, go back to the docket and refresh it to pull the newest information.
Your account does not support viewing this document.
You need a Paid Account to view this document. Click here to change your account type.
Your account does not support viewing this document.
Set your membership
status to view this document.
With a Docket Alarm membership, you'll
get a whole lot more, including:
- Up-to-date information for this case.
- Email alerts whenever there is an update.
- Full text search for other cases.
- Get email alerts whenever a new case matches your search.
One Moment Please
The filing “” is large (MB) and is being downloaded.
Please refresh this page in a few minutes to see if the filing has been downloaded. The filing will also be emailed to you when the download completes.
Your document is on its way!
If you do not receive the document in five minutes, contact support at support@docketalarm.com.
Sealed Document
We are unable to display this document, it may be under a court ordered seal.
If you have proper credentials to access the file, you may proceed directly to the court's system using your government issued username and password.
Access Government Site
